Eliaz Noam, Foucks Nitzan, Geva Dolev, Oren Shai, Shriki Noy, Vaknin Danielle, Fishman Dimitry, Levi Ofer
Biomaterials and Corrosion Lab, Department of Materials Science and Engineering, Tel-Aviv University, Ramat Aviv, Tel Aviv 6997801, Israel.
Materials Science and Engineering Division, Depot 22, Israel Air Force, P.O. Box 02538, Tel Aviv, Israel.
Materials (Basel). 2020 Sep 19;13(18):4171. doi: 10.3390/ma13184171.
Additive manufacturing attracts much interest for manufacturing and repair of structural parts for the aerospace industry. This paper presents comparative characterization of aircraft items made of Al 4047 alloy, Ti-6Al-4V alloy, and 17-4 precipitation hardened (PH) (AISI 630) stainless steel, either manufactured or repaired by laser engineered net shaping (LENS). Chemical analysis, density, and surface roughness measurements, X-ray micro-computed tomography (μ-CT) analysis, metallography, and micro-hardness testing were conducted. In all three materials, microstructures typical of rapid solidification were observed, along with high density, chemical composition, and hardness comparable to those of the counterpart wrought alloys (even in hard condition). High standard deviation in hardness values, anisotropic geometrical distortion, and overbuild at top edges were observed. The detected defects included partially melted and unmelted powder particles, porosity, and interlayer lack of fusion, in particular at the interface between the substrate plate and the build. There was a fairly good match between the density values measured by μ-CT and those measured by the Archimedes method; there was also good correlation between the type of defects detected by both techniques. Surface roughness, density of partially melted powder particles, and the content of bulk defects were significantly higher in Al 4047 than in 17-4 PH stainless steel and Ti-6Al-4V alloy. Optical gaging can be used reliably for surface roughness measurements. The implications of these findings are discussed.
增材制造在航空航天工业结构部件的制造和修复方面引起了广泛关注。本文介绍了由Al 4047合金、Ti-6Al-4V合金和17-4沉淀硬化(PH)(AISI 630)不锈钢制成的飞机部件的对比特性,这些部件通过激光工程净成形(LENS)制造或修复。进行了化学分析、密度和表面粗糙度测量、X射线微计算机断层扫描(μ-CT)分析、金相分析和显微硬度测试。在所有三种材料中,均观察到了典型的快速凝固微观结构,同时其密度、化学成分和硬度与对应的锻造合金相当(即使在硬态下)。观察到硬度值存在较高的标准偏差、各向异性几何变形以及顶部边缘的过度堆积。检测到的缺陷包括部分熔化和未熔化的粉末颗粒、孔隙率以及层间未熔合,特别是在基板与构建层之间的界面处。μ-CT测量的密度值与阿基米德法测量的密度值之间有相当好的匹配;两种技术检测到的缺陷类型之间也有良好的相关性。Al 4047的表面粗糙度、部分熔化粉末颗粒的密度和整体缺陷含量明显高于17-4 PH不锈钢和Ti-6Al-4V合金。光学测量可可靠地用于表面粗糙度测量。讨论了这些发现的意义。