Bryant S, Retief D H, Russell C M, Denys F R
Am J Orthod Dentofacial Orthop. 1987 Sep;92(3):225-31. doi: 10.1016/0889-5406(87)90416-1.
The purpose of this in vitro study was to determine the tensile bond strengths (TBS) of several orthodontic bonding systems and orthodontic brackets to enamel surfaces exposed to different etching procedures. The TBS of four bonding systems were determined by a test method developed by Kemper and Kilian. Twelve test specimens were prepared for each procedure. The test system was modified to determine the TBS of orthodontic brackets bonded to enamel surfaces by six bonding procedures and the TBS were evaluated 15 minutes and 24 hours after specimen preparation. The specimens were loaded to failure in an Instron machine operated at a crosshead speed of 0.02 inch/min. The TBS were expressed in MN.m-2. The TBS of the four bonding systems to etched enamel were not significantly different (P = 0.2528). The TBS of bonded brackets determined 24 hours after specimen preparation were not significantly different than the TBS recorded after 15 minutes except for brackets bonded with Lee Cleanse and Bond I to enamel surfaces etched with 15% H3PO4 for 30 seconds. The TBS of brackets to enamel etched with 15% H3PO4 for 30 seconds were not significantly different from the TBS to enamel surfaces etched with 5% H3PO4 for 15 seconds except for brackets bonded with Lee Cleanse and Bond II and tested 24 hours after bonding.
