Amorim Tatiane Lima, Duarte Lucas Mattos, da Silva Erick Mendes, de Oliveira Marcone Augusto Leal
Grupo de Química Analítica e Quimiometria (GQAQ), Departamento de Química, Universidade Federal de Juiz de Fora, Juiz de Fora, MG, Brazil.
Departamento de Química Analítica, Instituto de Química, Universidade Federal Fluminense, Niterói, RJ, Brazil.
Electrophoresis. 2021 Feb;42(3):289-304. doi: 10.1002/elps.202000260. Epub 2020 Nov 22.
Fatty acids determination is of paramount importance for quality control and suitable labeling of edible oils, required by regulatory agencies in several countries, and fast methods for this determination are worldly desired. This review article aimed to explore the available analytical methods for vegetable and marine oils analyses employing CE, which can be a straightforward and faster alternative than GC methods for fatty acid determination, considering some purposes. CE usually offers the possibility of a rapid analysis with a simple preparation of the sample, without requiring specific columns, which are inherent advantages of the technique. Instrumental conditions and the key points about fatty acids determination employing the technique are highlighted, and the main challenges and perspectives are also approached. Potential use of CE for edible oil analyses has been demonstrated for research and routine, which can be of interest for industries, regulatory agencies, and edible oil researchers. Therefore, we have explored the analytical approaches described in the last decades, intending to spread the interest of CE methods for fatty acid monitoring, label accuracy assessment, and food authenticity evaluation of edible oils.
脂肪酸测定对于食用油的质量控制和适当标签标注至关重要,这是多个国家监管机构的要求,因此全世界都渴望有快速的测定方法。这篇综述文章旨在探索采用毛细管电泳(CE)分析植物油和海洋油的可用分析方法,考虑到某些目的,对于脂肪酸测定而言,CE可能是比气相色谱(GC)方法更直接、更快的替代方法。CE通常提供了快速分析的可能性,样品制备简单,无需特定的色谱柱,这是该技术固有的优势。本文突出了使用该技术进行脂肪酸测定的仪器条件和关键点,同时也探讨了主要挑战和前景。CE在食用油分析中的潜在用途已在研究和常规分析中得到证明,这可能会引起行业、监管机构和食用油研究人员的兴趣。因此,我们探索了过去几十年中描述的分析方法,旨在传播CE方法在食用油脂肪酸监测、标签准确性评估和食品真实性评价方面的应用价值。