Godec M, Podgornik B, Kocijan A, Donik Č, Balantič D A Skobir
Institute of Metals and Technology, Lepi pot 11, 1000, Ljubljana, Slovenia.
Sci Rep. 2021 Feb 8;11(1):3277. doi: 10.1038/s41598-021-82572-y.
18Ni-300 maraging steel manufactured by selective laser melting was plasma nitrided to improve its wear and corrosion resistance. The effects of a prior solution treatment, aging and the combination of both on the microstructure and the properties after nitriding were investigated. The results were compared with conventionally produced 18Ni-300 counterparts subjected to the same heat- and thermo-chemical treatments. The plasma nitriding was performed under the same conditions (temperature of 520 °C and time of 6 h) as the aging in order to investigate whether the nitriding and the aging could be carried out simultaneously in a single step. The aim of this work was to provide a better understanding of the morphology and chemical composition of the nitrided layer in the additive-manufactured maraging steel as a function of the prior heat treatments and to compare the wear and corrosion resistance with those of conventional maraging steel. The results show that nitriding without any prior aging leads to cracks in the compound layer, while nitriding of the prior-heat-treated additive-manufactured maraging steel leads to benefits from the thermochemical treatment in terms of wear and corrosion resistance. Some explanations for the origins of the cracks and pores in the nitride layers are provided.
通过选择性激光熔化制造的18Ni-300马氏体时效钢进行了等离子渗氮处理,以提高其耐磨性和耐腐蚀性。研究了预先固溶处理、时效以及两者结合对渗氮后微观结构和性能的影响。将结果与经过相同热处理和热化学处理的传统生产的18Ni-300对应材料进行了比较。为了研究渗氮和时效是否可以在一个步骤中同时进行,在与时效相同的条件下(温度520°C,时间6小时)进行了等离子渗氮。这项工作的目的是更好地理解增材制造马氏体时效钢中渗氮层的形态和化学成分与预先热处理的关系,并将其耐磨性和耐腐蚀性与传统马氏体时效钢进行比较。结果表明,未经任何预先时效的渗氮会导致化合物层出现裂纹,而对预先热处理的增材制造马氏体时效钢进行渗氮,在耐磨性和耐腐蚀性方面会从热化学处理中受益。文中对氮化物层中裂纹和孔隙的产生原因提供了一些解释。