Tomiczek Błażej, Snopiński Przemysław, Borek Wojciech, Król Mariusz, Gutiérrez Ana Romero, Matula Grzegorz
Scientific and Didactic Laboratory of Nanotechnology and Material Technologies, Faculty of Mechanical Engineering, Silesian University of Technology, 44-100 Gliwice, Poland.
Department of Engineering Materials and Biomaterials, Silesian University of Technology, 18A Konarskiego Street, 44-100 Gliwice, Poland.
Materials (Basel). 2023 Mar 17;16(6):2412. doi: 10.3390/ma16062412.
In this article, hot compression tests on the additively produced 18Ni-300 maraging steel 18Ni-300 were carried out on the Gleeble thermomechanical simulator in a wide temperature range (900-1200 °C) and at strain rates of 0.001 10 s. The samples were microstructurally analysed by light microscopy and scanning electron microscopy with electron backscatter diffraction (EBSD). This showed that dynamic recrystallization (DRX) was predominant in the samples tested at high strain rates and high deformation temperatures. In contrast, dynamic recovery (DRV) dominated at lower deformation temperatures and strain rates. Subsequently, the material constants were evaluated in a constitutive relationship using the experimental flow stress data. The results confirmed that the specimens are well hot workable and, compared with the literature data, have similar activation energy for hot working as the conventionally fabricated specimens. The findings presented in this research article can be used to develop novel hybrid postprocessing technologies that enable single-stage net shape forging/forming of AM maraging steel parts at reduced forming forces and with improved density and mechanical properties.
在本文中,利用Gleeble热机械模拟器,在较宽的温度范围(900 - 1200°C)和0.001 - 10 s的应变速率下,对增材制造的18Ni - 300马氏体时效钢进行了热压缩试验。通过光学显微镜和配备电子背散射衍射(EBSD)的扫描电子显微镜对样品进行了微观结构分析。结果表明,在高应变速率和高变形温度下测试的样品中,动态再结晶(DRX)占主导地位。相比之下,在较低的变形温度和应变速率下,动态回复(DRV)占主导。随后,使用实验流动应力数据在本构关系中评估了材料常数。结果证实,这些试样具有良好的热加工性能,并且与文献数据相比,与传统制造的试样具有相似的热加工激活能。本文提出的研究结果可用于开发新型混合后处理技术,该技术能够在降低成型力的情况下,实现增材制造马氏体时效钢零件的单级净形锻造/成型,并提高密度和力学性能。