使用热固性聚合物合成的锌纳米颗粒的微观研究。
Microscopic study of zinc nanoparticles synthesised using thermosetting polymer.
作者信息
Tailor Giriraj, Chaudhay Jyoti, Verma Deepshikha, Kr Sarma Bhupendra
机构信息
Department of Polymer Science, M.L.S. University, Udaipur, Rajasthan, 313001, India.
Department of Chemistry, Mewar University, Chittorgarh, Rajasthan, 312901, India.
出版信息
Appl Microsc. 2019 Dec 31;49(1):20. doi: 10.1186/s42649-019-0018-0.
The present study reports the novel synthesis of Zinc nanoparticles (Zn NPs) by thermal decomposition method and its characterisation by Scanning Electron Microscope (SEM), Transmission Electron Microscope (TEM), and X-ray Diffraction Measurements (XRD). Synthesis of Zn NPs was achieved by using thermosetting polymer and zinc salts as precursor. Zn NPs were obtained on calcination at 850 °C for 30 min. SEM study reveals that synthesized nanoparticles are spherical in shape. XRD analysis shows that the Zn NPs formed are low crystalline in nature.
本研究报告了通过热分解法合成锌纳米颗粒（Zn NPs）的新方法及其通过扫描电子显微镜（SEM）、透射电子显微镜（TEM）和X射线衍射测量（XRD）进行的表征。通过使用热固性聚合物和锌盐作为前驱体实现了Zn NPs的合成。在850 °C煅烧30 min后获得了Zn NPs。SEM研究表明合成的纳米颗粒呈球形。XRD分析表明形成的Zn NPs本质上是低结晶的。
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