Hemes Susanne, Meiners Frank, Sizova Irina, Hama-Saleh Rebar, Röhrens Daniel, Weisheit Andreas, Häfner Constantin Leon, Bambach Markus
Access e.V., Intzestraße 5, 52072 Aachen, Germany.
Otto Fuchs KG, Derschlager Straße 26, 58540 Meinerzhagen, Germany.
Materials (Basel). 2021 Feb 22;14(4):1039. doi: 10.3390/ma14041039.
In the present study, we propose a hybrid manufacturing route to produce high-quality TiAlV parts, combining additive powder laser directed energy deposition (L-DED) for manufacturing of preforms, with subsequent hot forging as a thermomechanical processing (TMP) step. After L-DED, the material was hot formed at two different temperatures (930 °C and 1070 °C) and subsequently heat-treated for stress relief annealing. Tensile tests were performed on small sub-samples, taking into account different sample orientations with respect to the L-DED build direction and resulting in very good tensile strengths and ductility properties, similar or superior to the forged material. The resulting microstructure consists of very fine grained, partially globularized alpha grains, with a mean diameter ~0.8-2.3 µm, within a beta phase matrix, constituting between 2 and 9% of the sample. After forging in the sub-beta transus temperature range, the typical L-DED microstructure was no longer discernible and the anisotropy in tensile properties, common in additive manufacturing (AM), was significantly reduced. However, forging in the super-beta transus temperature range resulted in remaining anisotropies in the mechanical properties as well as an inferior tensile strength and ductility of the material. It was shown, that by combining L-DED with thermomechanical processing in the sub-beta transus temperature range of TiAlV, a suitable microstructure and desirable mechanical properties for many applications can be obtained, with the advantage of reducing the material waste.
在本研究中,我们提出了一种混合制造路线来生产高质量的TiAlV零件,该路线将用于制造预成型件的粉末激光定向能量沉积(L-DED)增材制造与随后作为热机械加工(TMP)步骤的热锻相结合。L-DED之后,材料在两个不同温度(930℃和1070℃)下进行热成型,随后进行消除应力退火的热处理。对小尺寸子样品进行拉伸试验,考虑到相对于L-DED构建方向的不同样品取向,结果显示出非常好的拉伸强度和延展性,与锻造材料相似或更优。所得微观结构由非常细的、部分球化的α晶粒组成,平均直径约为0.8-2.3μm,存在于β相基体中,占样品的2%-9%。在亚β转变温度范围内锻造后,典型的L-DED微观结构不再明显,增材制造(AM)中常见的拉伸性能各向异性显著降低。然而,在超β转变温度范围内锻造导致材料的力学性能仍存在各向异性,以及拉伸强度和延展性较差。结果表明,通过在TiAlV的亚β转变温度范围内将L-DED与热机械加工相结合,可以获得适用于许多应用的微观结构和理想的力学性能,同时具有减少材料浪费的优点。