Area of Food Technology, Faculty of Chemical Sciences and Technologies, Regional Institute for Applied Scientific Research (IRICA), University of Castilla-La Mancha, Avda. Camilo José Cela 10, 13071 Ciudad Real, Spain.
Area of Food Technology, Higher Technical School of Agronomic Engineering, University of Castilla-La Mancha, Ronda de Calatrava 7, 13071 Ciudad Real, Spain.
Molecules. 2021 Feb 23;26(4):1193. doi: 10.3390/molecules26041193.
This study presents the effect of the application of high-power ultrasound to crushed grapes, at a winery-scale, on the content of varietal volatile compounds (free and glycosidically-bound) in musts and on the overall aroma of wines. Two different frequencies (20 kHz and 28 kHz) were tested and the combination of grape sonication and different maceration times on wine aroma was also evaluated. The volatile compounds were isolated by solid phase extraction and analyzed by gas chromatography-mass spectrometry, carrying out a sensory evaluation of wines by quantitative descriptive analysis. Sonication produced an increase in the concentration of free varietal compounds such as C alcohols, terpenes and norisoprenoids in musts and also in wines made by 48 h of skin maceration, being less efficient in the extraction of the bound fraction. Fermentation compounds were also positively affected by ultrasound treatment, although this effect was variable depending on the frequency used, the maceration time and the type of compound. All the wines made from sonicated grapes had better scores in the evaluated olfactory attributes with respect to the control wines. Our results indicate that sonication could produce an increase in the content of some volatile compounds of sensory relevance, obtaining wines with an aroma quality similar or higher than those elaborated with longer maceration times.
本研究展示了在酿酒厂规模下,将高功率超声波应用于压碎的葡萄对葡萄汁中品种挥发性化合物(游离和糖苷结合)含量以及葡萄酒整体香气的影响。测试了两种不同的频率(20 kHz 和 28 kHz),并评估了葡萄超声处理和不同浸渍时间对葡萄酒香气的组合影响。通过固相萃取分离挥发性化合物,并通过气相色谱-质谱进行分析,通过定量描述分析对葡萄酒进行感官评价。超声处理使葡萄汁和浸渍 48 小时的皮中游离品种化合物(如 C 醇、萜烯和异戊二烯)的浓度增加,而对结合部分的提取效率较低。发酵化合物也受到超声处理的积极影响,尽管这种影响因使用的频率、浸渍时间和化合物类型而异。与对照酒相比,所有来自超声处理葡萄的葡萄酒在评估的嗅觉属性方面得分都更高。我们的结果表明,超声处理可以增加一些具有感官相关性的挥发性化合物的含量,从而获得具有类似于或高于长时间浸渍的香气质量的葡萄酒。