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Use of 2-methyl-(3,6-di-O-acetyl-1,2,4-trideoxy-4-fluoro-alpha-D- glucopyrano)-[2,1-d]-2-oxazoline as a glycosyl donor. Synthesis of benzyl 2-acetamido-6-O-(2-acetamido-2,4-dideoxy-4-fluoro-beta-D-glucopyran osy l)-2- deoxy-alpha-D-galactopyranoside.

作者信息

Thomas R L, Abbas S A, Matta K L

机构信息

Department of Gynecologic Oncology, Roswell Park Memorial Institute, New York State Department of Health, Buffalo 14263.

出版信息

Carbohydr Res. 1988 Apr 1;175(1):153-7. doi: 10.1016/0008-6215(88)80166-6.

DOI:10.1016/0008-6215(88)80166-6
PMID:3378238
Abstract
摘要

相似文献

1
Use of 2-methyl-(3,6-di-O-acetyl-1,2,4-trideoxy-4-fluoro-alpha-D- glucopyrano)-[2,1-d]-2-oxazoline as a glycosyl donor. Synthesis of benzyl 2-acetamido-6-O-(2-acetamido-2,4-dideoxy-4-fluoro-beta-D-glucopyran osy l)-2- deoxy-alpha-D-galactopyranoside.
Carbohydr Res. 1988 Apr 1;175(1):153-7. doi: 10.1016/0008-6215(88)80166-6.
2
The synthesis of allyl 2-acetamido-3,6-di-O-benzyl-2-deoxy-alpha-D-glucopyranoside and of chitobiose derivatives by the oxazoline procedure.通过恶唑啉法合成烯丙基 2-乙酰氨基-3,6-二-O-苄基-2-脱氧-α-D-吡喃葡萄糖苷和壳二糖衍生物。
Carbohydr Res. 1977 Jan;53(1):67-84. doi: 10.1016/s0008-6215(00)85455-5.
3
Synthesis of p-nitrophenyl 6-O-(2-acetamido-2-deoxy-beta-d-glucopyranosyl)-beta-D-galactopyranoside and p-nitrophenyl O-beta-D-galactopyranosyl-(1 linked to 3)-O-(2-acetamido-2-dexoy-beta-D-glucopyranosyl)-(1 linked to 6)-beta-D-galactopyranoside.6-O-(2-乙酰氨基-2-脱氧-β-D-吡喃葡萄糖基)-β-D-吡喃半乳糖苷对硝基苯酯和O-β-D-吡喃半乳糖基-(1→3)-O-(2-乙酰氨基-2-脱氧-β-D-吡喃葡萄糖基)-(1→6)-β-D-吡喃半乳糖苷对硝基苯酯的合成
Carbohydr Res. 1977 Feb;53(2):209-16. doi: 10.1016/s0008-6215(00)88088-x.
4
Synthetic mucin fragments. Methyl 6-O-(2-acetamido-2-deoxy-beta-D- glucopyranosyl)-beta-D-galactopyranoside, methyl 3,4-di-O-(2-acetamido-2-deoxy- beta-D-glucopyranosyl)-beta-D-galactopyranoside, and methyl O-(2-acetamido-2- deoxy-beta-D-glucopyranosyl)-(1----3)-O-beta-D-galactopyranosyl-(1---- 3)-O-(2- acetamido-2-deoxy-beta-D-glucopyranosyl)-(1----3)-beta-D-galactopyr ano side.合成粘蛋白片段。6-O-（2-乙酰氨基-2-脱氧-β-D-吡喃葡萄糖基）-β-D-吡喃半乳糖苷甲酯、3,4-二-O-（2-乙酰氨基-2-脱氧-β-D-吡喃葡萄糖基）-β-D-吡喃半乳糖苷甲酯和O-（2-乙酰氨基-2-脱氧-β-D-吡喃葡萄糖基）-（1→3）-O-β-D-吡喃半乳糖基-（1→3）-O-（2-乙酰氨基-2-脱氧-β-D-吡喃葡萄糖基）-（1→3）-β-D-吡喃半乳糖苷甲酯。
Carbohydr Res. 1987 Mar 15;161(1):39-47. doi: 10.1016/0008-6215(87)84004-1.
5
Synthetic mucin fragments. Benzyl O-(2-acetamido-2-deoxy-alpha-D-glucopyranosyl)-(1----3)-O-beta-D- galactopyranosyl-(1----3)-O-[(2-acetamido-2-deoxy-beta-D-glucopyran osy l)- (1----6)]-2-acetamido-2-deoxy-alpha-D-galactopyranoside and benzyl O-(2-acetamido-2-deoxy-beta-D-glucopyranosyl)-(1----3)-O-beta-D- galactopyranosyl-(1----3)-O-[beta-D-galactopyranosyl-(1----6)]-2-ac eta mido- 2-deoxy-alpha-D-galactopyranoside.合成粘蛋白片段。苄基 O-(2-乙酰氨基-2-脱氧-α-D-吡喃葡萄糖基)-(1→3)-O-β-D-吡喃半乳糖基-(1→3)-O-[(2-乙酰氨基-2-脱氧-β-D-吡喃葡萄糖基)-(1→6)]-2-乙酰氨基-2-脱氧-α-D-吡喃半乳糖苷和苄基 O-(2-乙酰氨基-2-脱氧-β-D-吡喃葡萄糖基)-(1→3)-O-β-D-吡喃半乳糖基-(1→3)-O-[β-D-吡喃半乳糖基-(1→6)]-2-乙酰氨基-2-脱氧-α-D-吡喃半乳糖苷。
Carbohydr Res. 1988 Dec 1;183(2):163-73. doi: 10.1016/0008-6215(88)84071-0.
6
Synthesis of benzyl 2-acetamido-2-deoxy-3-O-beta-D-fucopyranosyl-alpha-D-galactopyranoside and benzyl 2-acetamido-6-O-(2-acetamido-2-deoxy-beta- D-glucopyranosyl)-2-deoxy-3-O-beta-D-fucopyranosyl-alpha-D- galactopyranoside.2-乙酰氨基-2-脱氧-3-O-β-D-岩藻糖基-α-D-吡喃半乳糖苷苄酯和2-乙酰氨基-6-O-(2-乙酰氨基-2-脱氧-β-D-吡喃葡萄糖基)-2-脱氧-3-O-β-D-岩藻糖基-α-D-吡喃半乳糖苷苄酯的合成
Carbohydr Res. 1984 Aug 15;131(2):257-63. doi: 10.1016/0008-6215(84)85247-7.
7
Synthetic mucin fragments: benzyl 2-acetamido-6-O-(2-acetamido-2-deoxy-beta- D-glucopyranosyl)-2-deoxy-3-O-beta-D-galactopyranosyl-alpha-D- galactopyranoside and benzyl 2-acetamido-6-O-(2-acetamido-2-deoxy-beta-D-glucopyranosyl)- 3-O-[6-O-(2-acetamido-2-deoxy-beta-D-glucopyranosyl)-beta-D- galactopyranosyl]-2-deoxy-alpha-D-galactopyranoside.合成粘蛋白片段：苄基2-乙酰氨基-6-O-（2-乙酰氨基-2-脱氧-β-D-吡喃葡萄糖基）-2-脱氧-3-O-β-D-吡喃半乳糖基-α-D-吡喃半乳糖苷和苄基2-乙酰氨基-6-O-（2-乙酰氨基-2-脱氧-β-D-吡喃葡萄糖基）-3-O-[6-O-（2-乙酰氨基-2-脱氧-β-D-吡喃葡萄糖基）-β-D-吡喃半乳糖基]-2-脱氧-α-D-吡喃半乳糖苷。
Carbohydr Res. 1984 Mar 1;126(1):115-24. doi: 10.1016/0008-6215(84)85130-7.
8
Synthesis of 2-methyl-[2-acetamido-4-O-acetyl-6-O-benzyl-3-O-(2-butenyl)-1,2-dideoxy-alpha-D -glucopyrano]-[2,1-d]-2-oxazoline, a versatile intermediate for the synthesis of complex oligosaccharides of bacterial cell-wall, human milk, and blood-group substances.2-甲基-[2-乙酰氨基-4-O-乙酰基-6-O-苄基-3-O-(2-丁烯基)-1,2-二脱氧-α-D-吡喃葡萄糖基]-[2,1-d]-2-恶唑啉的合成，一种用于合成细菌细胞壁、人乳和血型物质复杂寡糖的通用中间体。
Carbohydr Res. 1981 Mar 2;89(2):279-88. doi: 10.1016/s0008-6215(00)85253-2.
9
Preparation of 4,6-cyclo-hexopyranoses by palladium-mediated intramolecular cyclodehalogenation.
Carbohydr Res. 1993 Jul 19;245(2):233-44. doi: 10.1016/0008-6215(93)80074-o.
10
The synthesis of a trisaccharide and a tetrasaccharide lipid intermediate. P1-dolichyl P2-[O-beta-D-mannopyranosyl-(1----4)-O-(2-acetamido-2-deoxy- beta-D-glucopyranosyl)-(1----4)-2-acetamido-2-deoxy-alpha-D- glucopyranosyl] diphosphate and P1-dolichyl P2-[O-alpha-D-mannopyranosyl-(1----3)-O-beta-D- mannopyranosyl-(1----4)-O-(2-acetamido-2-deoxy-beta-D-glucopyranosyl)- (1----4)-2-acetamido-2-deoxy-alpha-D-glucopyranosyl] diphosphate.一种三糖和一种四糖脂质中间体的合成。P1-多萜醇P2-[O-β-D-甘露吡喃糖基-(1→4)-O-(2-乙酰氨基-2-脱氧-β-D-葡萄糖吡喃糖基)-(1→4)-2-乙酰氨基-2-脱氧-α-D-葡萄糖吡喃糖基]二磷酸酯和P1-多萜醇P2-[O-α-D-甘露吡喃糖基-(1→3)-O-β-D-甘露吡喃糖基-(1→4)-O-(2-乙酰氨基-2-脱氧-β-D-葡萄糖吡喃糖基)-(1→4)-2-乙酰氨基-2-脱氧-α-D-葡萄糖吡喃糖基]二磷酸酯。
Carbohydr Res. 1984 Mar 1;126(1):61-80. doi: 10.1016/0008-6215(84)85126-5.

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