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通过放电等离子烧结制备的铝基纳米复合材料的电导率增强

Enhancement of Electrical Conductivity of Aluminum-Based Nanocomposite Produced by Spark Plasma Sintering.

作者信息

Ulloa-Castillo Nicolás A, Hernández-Maya Roberto, Islas-Urbano Jorge, Martínez-Romero Oscar, Segura-Cárdenas Emmanuel, Elías-Zúñiga Alex

机构信息

Tecnologico de Monterrey, Department of Mechanical Engineering and Advanced Materials, School of Engineering and Sciences, Av. Eugenio Garza Sada Sur 2501, Monterrey 64849, Nuevo León, Mexico.

Siemens, Research and Development Department, Libramiento Arco Vial Poniente Km 4.2, Santa Catarina 66350, Nuevo León, Mexico.

出版信息

Nanomaterials (Basel). 2021 Apr 28;11(5):1150. doi: 10.3390/nano11051150.

Abstract

This article focuses on exploring how the electrical conductivity and densification properties of metallic samples made from aluminum (Al) powders reinforced with 0.5 wt % concentration of multi-walled carbon nanotubes (MWCNTs) and consolidated through spark plasma sintering (SPS) process are affected by the carbon nanotubes dispersion and the Al particles morphology. Experimental characterization tests performed by scanning electron microscopy (SEM) and by energy dispersive spectroscopy (EDS) show that the MWCNTs were uniformly ball-milled and dispersed in the Al surface particles, and undesirable phases were not observed in X-ray diffraction measurements. Furthermore, high densification parts and an improvement of about 40% in the electrical conductivity values were confirmed via experimental tests performed on the produced sintered samples. These results elucidate that modifying the powder morphology using the ball-milling technique to bond carbon nanotubes into the Al surface particles aids the ability to obtain highly dense parts with increasing electrical conductivity properties.

摘要

本文重点探讨通过火花等离子烧结(SPS)工艺固结的、由含0.5 wt%多壁碳纳米管(MWCNT)增强的铝(Al)粉末制成的金属样品的电导率和致密化特性,是如何受到碳纳米管分散情况和铝颗粒形态的影响。通过扫描电子显微镜(SEM)和能量色散光谱(EDS)进行的实验表征测试表明,MWCNT被均匀球磨并分散在铝表面颗粒中,且在X射线衍射测量中未观察到不良相。此外,通过对所制备的烧结样品进行实验测试,证实了高致密化部件以及电导率值提高约40%。这些结果表明,使用球磨技术改变粉末形态,将碳纳米管结合到铝表面颗粒中,有助于获得具有更高电导率特性的高密度部件。

https://cdn.ncbi.nlm.nih.gov/pmc/blobs/6074/8170884/0f0d3835d19d/nanomaterials-11-01150-g001.jpg

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