Department of Food Science and Engineering, School of Agricultural Engineering and Food Sciences, Shandong University of Technology, Zibo, China.
School of Agriculture and Food, The University of Melbourne, Parkville, Australia.
J Sci Food Agric. 2021 Dec;101(15):6239-6247. doi: 10.1002/jsfa.11290. Epub 2021 May 20.
A material's physical and chemical properties during drying are influenced by water status and distribution. However, merely overall water removal is reported in many investigations, which hinders clarification of the drying mechanism. Therefore, the effects of ultrasound (US) pretreatment (0 W, CK; 90 W, US-90; 180 W, US-180) on the drying kinetics and quality of heat pump drying (HPD) scallop adductors was performed based on low-field nuclear magnetic resonance (LF-NMR).
Compared with CK, effective moisture diffusion coefficient was increased by 12.43% and 23.35% for US-90 and US-180, respectively. The Weibull model satisfactorily described the drying characteristics with a high r (> 0.998), low rmse (< 0.0120) and χ (< 0.00008). LF-NMR revealed that the immobilized water was predominant in scallop adductors. As drying proceeded, the relaxation time of free and immobilized water was decreased sharply, whereas the relaxation time of bound water scarcely changed. The time required to reduce approximately two-fifths of the original peak area of immobilized water was 720, 630 and 540 min for CK, US-90 and US-180, respectively. The amplitude of immobilized water was decreased and bound water increased significantly, although free water was kept constant (ranging 1-2%). US pretreatment reduced total color difference and hardness, but enhanced the toughness of dried scallop adductors. However, US had no significant influence on the product rehydration rate and shrinkage rate.
LF-NMR was successfully employed to evaluate the drying degree of scallop adductors. US facilitated the conversion of immobilized water to free water and, consequently, promoted water removal during HPD. © 2021 Society of Chemical Industry.
干燥过程中材料的物理和化学性质受水分状态和分布的影响。然而,许多研究仅仅报道了总的水分去除情况,这阻碍了干燥机理的澄清。因此,基于低场核磁共振(LF-NMR),研究了超声(US)预处理(0 W,CK;90 W,US-90;180 W,US-180)对热泵干燥(HPD)扇贝附肢干燥动力学和品质的影响。
与 CK 相比,US-90 和 US-180 的有效水分扩散系数分别提高了 12.43%和 23.35%。Weibull 模型很好地描述了干燥特性,r 值高(>0.998),rmse 值低(<0.0120),χ 值低(<0.00008)。LF-NMR 表明,扇贝附肢中主要存在束缚水。随着干燥的进行,自由水和束缚水的弛豫时间急剧下降,而结合水的弛豫时间几乎不变。减少束缚水原始峰面积约五分之二所需的时间分别为 CK、US-90 和 US-180 的 720、630 和 540 min。尽管自由水保持不变(1-2%),但束缚水的幅度减小,结合水增加,超声预处理显著降低了总色差和硬度,提高了干燥扇贝附肢的韧性。然而,US 对产品复水率和收缩率没有显著影响。
LF-NMR 成功地用于评估扇贝附肢的干燥程度。US 促进了束缚水向自由水的转化,从而促进了 HPD 过程中的水分去除。© 2021 化学工业协会。