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尼龙增强结构与牙科树脂之间的粘结强度分析

Analysis of bond strength between a nylon reinforcement structure and dental resins.

作者信息

Nakano Leonardo-Jiro-Nomura, Lopes Guilherme-da Rocha-Scalzer, Firmino Aline-Silva, de Matos Jefferson-David-Melo, Tango Rubens-Nisie, Paes-Junior Tarcisio-José-de Arruda

机构信息

Department of Prosthodontics and Dental Materials, São Paulo State University (Unesp) - Institute of Science and Technology, São José dos Campos - SP, Brazil.

Department of Dentistry, Universidade São Francisco UFS, Bragança Paulista - SP, Brazil.

出版信息

J Clin Exp Dent. 2021 May 1;13(5):e505-e510. doi: 10.4317/jced.57654. eCollection 2021 May.

Abstract

BACKGROUND

Nylon is a polymer that its use to reinforce dental resins has shown positive results such as increased flexural strength. The aim of this study was to evaluate the bond strength between dental resins and a nylon reinforcement.

MATERIAL AND METHODS

Forty cylindrical nylon blocks with 13 x 23 mm with 0.5% by volume of silica and 40 without were made. Half of the samples of each nylon composition were sandblasted with aluminum oxide (50μm) for 3 s (2.8 bar pressure, distance: 20 mm, incidence angle: 90o). On the nylon blocks, cylinders of chemically activated acrylic resin and indirect composite resin were made, with a bonding area of 6,28 mm2. Eight different groups were obtained according to the material used and the surface treatment (n = 10): Acrylic Resin + Nylon; GAS: Acrylic Resin + Nylon with Silica; GAT: Acrylic Resin + Nylon (Al2O3); GAST: Acrylic Resin + Nylon with Silica (Al2O3); GC: Composite Resin + Nylon; GCS: Composite Resin + Nylon with Silica; GCT: Composite Resin + Nylon (Al2O3); GCST: Composite Resin + Nylon with Silica (Al2O3). The shear test was carried out. The Student's and the Kruskal-Wallis test was adopted.

RESULTS

There was no statistically difference in the bond strength for nylon with silica for the acrylic resin group. For the composite groups, nylon with silica did not present a statistically difference without surface treatment ( = 0.10) and with surface treatment the bond strength decreased ( = 0.000). The GCT showed a higher bond strength (0.89 MPa). The surface treatment improved the bond strength for the both groups.

CONCLUSIONS

The presence of silica in the nylon composition did not influence the bond strength between materials evaluated. However, the surface treatment with aluminum oxide proved to be favorable for this adhesion. Nylons - Resins, Synthetic - Structures Strengthening - Dental Research.

摘要

背景

尼龙是一种聚合物,其用于增强牙科树脂已显示出积极效果,如提高弯曲强度。本研究的目的是评估牙科树脂与尼龙增强材料之间的粘结强度。

材料与方法

制作了40个直径13×23mm、含0.5%(体积)二氧化硅的圆柱形尼龙块和40个不含二氧化硅的尼龙块。每种尼龙组合物的一半样品用氧化铝(50μm)喷砂3秒(气压2.8巴,距离20mm,入射角90°)。在尼龙块上制作化学活化丙烯酸树脂和间接复合树脂圆柱体,粘结面积为6.28mm²。根据所用材料和表面处理方式获得8个不同组(n = 10):丙烯酸树脂+尼龙;GAS:含二氧化硅的丙烯酸树脂+尼龙;GAT:丙烯酸树脂+尼龙(氧化铝处理);GAST:含二氧化硅的丙烯酸树脂+尼龙(氧化铝处理);GC:复合树脂+尼龙;GCS:含二氧化硅的复合树脂+尼龙;GCT:复合树脂+尼龙(氧化铝处理);GCST:含二氧化硅的复合树脂+尼龙(氧化铝处理)。进行剪切试验。采用学生 t 检验和克鲁斯卡尔 - 沃利斯检验。

结果

丙烯酸树脂组中含二氧化硅的尼龙粘结强度无统计学差异。对于复合树脂组,未进行表面处理时含二氧化硅的尼龙无统计学差异(P = 0.10),进行表面处理后粘结强度降低(P = 0.000)。GCT组显示出较高的粘结强度(0.89MPa)。表面处理提高了两组的粘结强度。

结论

尼龙组合物中二氧化硅的存在不影响所评估材料之间的粘结强度。然而,氧化铝表面处理被证明有利于这种粘结。尼龙 - 树脂,合成材料 - 结构增强 - 牙科研究

https://cdn.ncbi.nlm.nih.gov/pmc/blobs/df84/8106934/ea2f35d878e4/jced-13-e505-g001.jpg

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