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冷大气等离子体提高饰面复合材料与氧化锆的剪切粘结强度。

Cold Atmospheric Plasma Improves Shear Bond Strength of Veneering Composite to Zirconia.

作者信息

Bunz Oskar, Kalz Paul, Benz Carla I, Naumova Ella A, Arnold Wolfgang H, Piwowarczyk Andree

机构信息

Department of Prosthodontics, School of Dentistry, Faculty of Health, Witten/Herdecke University, 58455 Witten, Germany.

Private Practice, 45128 Essen, Germany.

出版信息

Dent J (Basel). 2021 May 21;9(6):59. doi: 10.3390/dj9060059.

Abstract

Chipping of veneering is the most common clinical complication for zirconia restorations. Veneering composite could be a promising alternative to renew restorations. Zirconia discs (3-YSZ) were prepared with varying surface treatments and bonded to indirect composite as follows: air abrasion and Scotchbond Universal (A/SU); air abrasion and Clearfil Ceramic Primer (A/C); air abrasion and MKZ Primer (A/M); air abrasion and Monobond Plus (A/MP); silica-coating and Scotchbond Universal (S/SU); air abrasion (AP/SU), additional cold atmospheric plasma treatment, and Scotchbond Universal. An indirect composite material was then applied to the zirconia specimens. Specimens were divided into subgroups for short-term (14 days storage at 37 °C and 5000 thermal cycles) and long-term (250 days storage and 37,500 thermal cycles) artificial aging. Shear bond strength measurement (SBS) was performed, and data were analyzed by Kruskal-Wallis-test and multiple comparison testing with Dunn's correction ( ≤ 0.05). The median SBS values (MPa) of short- and long-term artificial aging were: 3.09/1.36 (A/SU); 0.77/1.43 (S/SU); 2.82/2.15 (AP/SU); 1.97/1.80 (A/C); 2.01/1.58 (A/M); and 1.70/1.68 (A/MP). For short-term artificial aging A/SU showed the highest median SBS values, whereas in the long-term trial, AP/SU showed the highest values and the difference was significant. A prolonged artificial aging decreased SBS in all groups, except S/SU. In summary, treatment with CAP can improve SBS in the long-term.

摘要

氧化锆修复体中贴面崩裂是最常见的临床并发症。贴面复合材料可能是修复修复体的一种有前景的替代方法。制备了经过不同表面处理的氧化锆盘(3-YSZ),并按如下方式与间接复合材料粘结:空气磨蚀和3M Scotchbond Universal粘结剂(A/SU);空气磨蚀和可乐丽Clearfil Ceramic Primer粘结剂(A/C);空气磨蚀和MKZ Primer粘结剂(A/M);空气磨蚀和可乐丽Monobond Plus粘结剂(A/MP);二氧化硅涂层和3M Scotchbond Universal粘结剂(S/SU);空气磨蚀(AP/SU)、额外的冷大气等离子体处理以及3M Scotchbond Universal粘结剂。然后将间接复合材料应用于氧化锆试件。将试件分为短期(在37℃下储存14天和进行5000次热循环)和长期(储存250天和进行37500次热循环)人工老化的亚组。进行剪切粘结强度测量(SBS),并通过Kruskal-Wallis检验和采用Dunn校正的多重比较检验(≤0.05)对数据进行分析。短期和长期人工老化的SBS中位数(MPa)分别为:3.09/1.36(A/SU);0.77/1.43(S/SU);2.82/2.15(AP/SU);1.97/1.80(A/C);2.01/1.58(A/M);以及1.70/1.68(A/MP)。对于短期人工老化,A/SU显示出最高的SBS中位数,而在长期试验中,AP/SU显示出最高值且差异显著。除S/SU外,延长人工老化会降低所有组的SBS。总之,冷大气等离子体处理在长期内可提高SBS。

https://cdn.ncbi.nlm.nih.gov/pmc/blobs/4e99/8224273/451b581a36b8/dentistry-09-00059-g001.jpg

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