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预拌混凝土质量评估中的实验室间对比试验

Interlaboratory Comparative Tests in Ready-Mixed Concrete Quality Assessment.

作者信息

Skrzypczak Izabela, Leśniak Agnieszka, Ochab Piotr, Górka Monika, Kokoszka Wanda, Sikora Anna

机构信息

Faculty of Civil and Environmental Engineering and Architecture, Rzeszow University of Technology, Powstancow Warszawy 12, 35-082 Rzeszow, Poland.

Faculty of Civil Engineering, Cracow University of Technology, 31-155 Krakow, Poland.

出版信息

Materials (Basel). 2021 Jun 22;14(13):3475. doi: 10.3390/ma14133475.

Abstract

Proper quality assessment of ready-mixed concrete, which is currently the principal material for construction, land engineering and architecture, has an impact on the optimisation and verification of correct functioning of individual stages of the production process. According to the European Standard EN 206 "Concrete-Specification, performance, production and conformity", obligatory conformity control of concrete is carried out by the producer during its production. In order to verify the quality of concrete, investors generally commission independent laboratory units to perform quality assessment of both concrete mix and hardened concrete, which guarantees a high quality of construction works. One of the essential tools for ensuring the quality of test results is the participation of laboratories in the so-called proficiency testing (PT) or inter-laboratory comparisons (ILC). Participation in PT/ILC programmes is, on the one hand, a tool for demonstrating the laboratory's performance, on the other hand an aid for maintaining the quality of available concrete tests and validating test methods. Positive evaluation is a confirmation of the laboratory's capability for performing the tests. The paper presents the results of laboratory proficiency tests carried out by means of inter-laboratory comparisons, as shown in the example of quality assessment of ready-mixed concrete for nine participating laboratories. The tests were performed for concrete of the following parameters: strength class C30/37, consistency S3, frost resistance degree F150, and water resistance degree W8. This involved determining consistencies, air content and density of the concrete mix, and compressive strength of hardened concrete. For the evaluation of laboratory performance results, , and were applied. The innovation of the proposed study lies in employing both classical and iterative robust statistical methods. In comparison with classical statistical methods, robust methods ensure a smaller impact of outliers and other anomalies on the measurement results. Following the analyses, clear differences were found between the types of detected discrepancy of test results, which occurred due to the nature of individual parameters. For two laboratories, two scores revealed unsatisfactory results for concrete mix consistency. The main reasons can be pouring into the cone-shaped form a concrete mixture that is too dry, or incorrect use of a measuring tool also creating a possibility that the obtained value can be wrongly recorded. Other possible reasons are discussed in the paper. Participation in inter-laboratory comparison programmes is undoubtedly a way to verify and raise the quality of tests performed for concrete mix and hardened concrete, whereas individual analysis of the results allows the laboratory quality system to be improved.

摘要

预拌混凝土是目前建筑、土地工程和建筑领域的主要材料,对其进行恰当的质量评估会影响生产过程各个阶段正确运行的优化和验证。根据欧洲标准EN 206《混凝土——规范、性能、生产与合格评定》,生产商在生产过程中要对混凝土进行强制性合格控制。为了验证混凝土质量,投资方通常委托独立实验室对混凝土拌和物和硬化混凝土进行质量评估,这能确保建筑工程的高质量。确保测试结果质量的关键工具之一是实验室参与所谓的能力验证测试(PT)或实验室间比对(ILC)。参与PT/ILC计划,一方面是展示实验室性能的工具,另一方面有助于维持现有混凝土测试的质量并验证测试方法。得到肯定评价是对实验室进行测试能力的确认。本文展示了通过实验室间比对进行的实验室能力验证测试结果,以九个参与实验室对预拌混凝土质量评估为例。针对以下参数的混凝土进行了测试:强度等级C30/37、稠度S3、抗冻性等级F150和抗渗性等级W8。这包括测定混凝土拌和物的稠度、含气量和密度,以及硬化混凝土的抗压强度。为评估实验室性能结果,应用了 、 和 。本研究的创新之处在于同时采用经典和迭代稳健统计方法。与经典统计方法相比,稳健方法能确保异常值和其他异常情况对测量结果的影响更小。经过分析,发现由于各个参数的性质,检测到的测试结果差异类型存在明显差异。对于两个实验室,两项得分显示混凝土拌和物稠度的结果不理想。主要原因可能是将过于干燥的混凝土混合料倒入锥形模具中,或者测量工具使用不当,也可能导致记录的数值有误。本文还讨论了其他可能的原因。参与实验室间比对计划无疑是验证和提高混凝土拌和物及硬化混凝土测试质量的一种方式,而对结果进行单独分析有助于改进实验室质量体系。

https://cdn.ncbi.nlm.nih.gov/pmc/blobs/b10d/8269485/a1029e5e10c2/materials-14-03475-g001.jpg

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