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实验室间比对作为产品评估过程的信息来源。瓷砖胶粘剂案例研究

Interlaboratory Comparison as a Source of Information for the Product Evaluation Process. Case Study of Ceramic Tiles Adhesives.

作者信息

Stancu Cristina, Michalak Jacek

机构信息

Ceprocim S.A., 6, Blvd. Preciziei, Sector 6, 062203 Bucharest, Romania.

Research and Development Center, Atlas sp. z o.o., 2, Kilińskiego St., 91-421 Lodz, Poland.

出版信息

Materials (Basel). 2021 Dec 29;15(1):253. doi: 10.3390/ma15010253.

Abstract

In this study, the results obtained by 19 laboratories participating in 2 editions of the interlaboratory comparison (ILC) determining 2 properties of ceramic tiles adhesives (CTAs), i.e., initial tensile adhesion strength and tensile adhesion strength after water immersion following EN 12004, were analyzed. The results show that participating laboratories maintain a constant quality of their work. The use of z-score analysis, under ISO 13528, allows for classifying 89.5% to 100% of laboratories as satisfactory, depending on the measurement's kind and edition. The remaining laboratories are classified as questionable. The investigation of the predominant mode of failure of the CTA's samples tested in the two editions shows significant differences. From the perspective of laboratories, the goal of the ILC has been achieved. From the standpoint of a manufacturer who evaluates a product's properties when placing it on the market, the results indicate the necessity of a particular treatment of the product evaluation process because the variability of the obtained results is significant. It increases the possibility of the product failing to meet the assessment criteria verified by the construction market supervision authorities. The manufacturer must consider all possible variations in the risk analysis, including the ILC results, to improve the assessment process of CTAs.

摘要

在本研究中,分析了19个实验室参与两版实验室间比对(ILC)所获得的结果,该比对依据EN 12004测定瓷砖胶粘剂(CTA)的两项性能,即初始拉伸粘结强度和浸水后的拉伸粘结强度。结果表明,参与实验室的工作质量保持稳定。根据ISO 13528进行的z分数分析显示,根据测量类型和版本不同,89.5%至100%的实验室被归类为满意。其余实验室被归类为有问题。对两版中测试的CTA样品的主要失效模式进行的调查显示出显著差异。从实验室的角度来看,ILC的目标已经实现。从制造商在产品投放市场时评估产品性能的角度来看,结果表明有必要对产品评估过程进行特殊处理,因为所获得结果的变异性很大。这增加了产品无法满足建筑市场监管当局验证的评估标准的可能性。制造商必须在风险分析中考虑所有可能的变化,包括ILC结果,以改进CTA的评估过程。

https://cdn.ncbi.nlm.nih.gov/pmc/blobs/2c40/8745809/f4d73d912aa3/materials-15-00253-g001.jpg

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