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生物模板法制备的还原氧化石墨烯的结构与形态表征及其抗菌效果

Structural and Morphological Characterization of Bio-templated Reduced Graphene Oxide and their Antibacterial Efficacy.

作者信息

Sethumadhavan Smina Chappalathottil, Pottail Lalitha, Sharma S C, Chithambharan Akhila, Ballal Suhas

机构信息

Department of Chemistry, Avinashilingam Institute for Home Science and Higher Education for Women, Coimbatore, Tamil Nadu India.

Department of Chemistry and Coordinator, Bharat Ratna Prof. C.N.R Rao Research Center, Avinashilingam Institute for Home Science and Higher Education for Women, Coimbatore, Tamil Nadu India.

出版信息

J Clust Sci. 2022;33(5):1997-2008. doi: 10.1007/s10876-021-02120-6. Epub 2021 Jul 6.

Abstract

We would like to report the eco-friendly synthesis of reduced graphene oxide using aqueous extract of (rhizome), dried fruit and seed parts of and the whole shell part of by simple steam bath technique. The structural and morphological characteristics of prepared reduced graphene oxides were determined by UV-Visible spectroscopy, Fourier Transform Infra-Red spectroscopy (FTIR), Field Emission Scanning Electron Microscopy (FESEM) and Raman spectroscopy. The Surface Plasmon Resonance at 260-280 nm ensured the reduced graphene oxide formation. The antibacterial efficacy of synthesized reduced graphene oxide was evaluated against both gram-positive and gram-negative pathogens such as and Among the selected samples mediated reduced graphene oxide showed excellent inhibition efficiency (27 and 28 mm) against and , respectively as compared to the standard Gentamycin (29 mm). showed significant inhibition of 22 mm and moderate inhibition of 18 mm against and , respectively The results suggest selected plants and chank shell-mediated reduced graphene oxide as potential antibacterial agents for various therapeutic applications.

摘要

我们想要报告通过简单的蒸汽浴技术,使用(根茎)的水提取物、(植物名)的干果和种子部分以及(植物名)的整个外壳部分来进行环保合成还原氧化石墨烯的方法。通过紫外可见光谱、傅里叶变换红外光谱(FTIR)、场发射扫描电子显微镜(FESEM)和拉曼光谱来确定所制备的还原氧化石墨烯的结构和形态特征。在260 - 280纳米处的表面等离子体共振确保了还原氧化石墨烯的形成。评估了合成的还原氧化石墨烯对革兰氏阳性和革兰氏阴性病原体(如(病原体名)和(病原体名))的抗菌效果。在所选择的样品中,(植物名)介导的还原氧化石墨烯对(病原体名)和(病原体名)分别表现出优异的抑制效率(27毫米和28毫米),相比标准庆大霉素(29毫米)。(植物名)对(病原体名)显示出22毫米的显著抑制和对(病原体名)18毫米的中度抑制。结果表明所选择的植物和贝壳介导的还原氧化石墨烯作为各种治疗应用的潜在抗菌剂。

https://cdn.ncbi.nlm.nih.gov/pmc/blobs/5b32/8260015/fa9e802b81f5/10876_2021_2120_Fig1_HTML.jpg

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