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三种半透明氧化钇稳定四方氧化锆多晶体与二硅酸锂微晶玻璃材料的光学和晶体特性比较。

Comparison of optical and crystal properties of three translucent yttria-stabilized tetragonal zirconia polycrystals with those of lithium disilicate glass-ceramic material.

作者信息

Wang Chun-Cheng, Fu Po-Sung, Wang Jen-Chyan, Lan Ting-Hsun, Lai Pei-Ling, Du Je-Kang, Chen Wen-Cheng, Hung Chun-Cheng

机构信息

School of Dentistry, College of Dental Medicine, Kaohsiung Medical University, Kaohsiung, Taiwan.

Department of Dentistry, Kaohsiung Municipal Ta-Tung Hospital, Kaohsiung, Taiwan.

出版信息

J Dent Sci. 2021 Oct;16(4):1247-1254. doi: 10.1016/j.jds.2021.01.004. Epub 2021 Jan 29.

Abstract

BACKGROUND/PURPOSE: Among the ceramic materials used for all-ceramic crowns, zirconia has high biocompatibility and favorable mechanical properties, but its main drawbacks include low translucency and stress-induced phase transformation. To stabilize high-strength tetragonal zirconia polycrystal (TZP), 3-5 mol% yttria is usually added to prepare yttria-stabilized TZP (Y-TZP). In this study, the optical properties of three commercial Y-TZP ceramics were compared with those of the clinically available glass-ceramic material of lithium disilicate, and the relationship between translucency and crystal properties was analyzed in vitro.

MATERIALS AND METHODS

Twelve 5-mm-thick standardized disks were prepared from three Y-TZP ceramics and one lithium disilicate block. Absolute translucency was measured using a spectrophotometer with an integrating sphere. X-ray diffraction was used to quantify the main structural parameters (i.e., preferred plane, quantitative phase, and grain size) of Y-TZP crystals.

RESULTS

The product-dominated phase of Y-TZP exhibited a tetragonal lattice pattern, and the preferred planes had minor variations. The diffraction patterns of the three Y-TZP ceramics demonstrated minor effects on translucency, without significant differences ( > 0.05). The grain size of 54-70 nm was negatively related to translucency in Y-TZP. Lithium disilicate specimens had significantly higher translucency than the three Y-TZP specimens ( < 0.001).

CONCLUSION

Grain size reduction played an essential role in developing highly translucent Y-TZP ceramics. The three Y-TZP ceramics were essentially opaque but exhibited poorer translucency than lithium disilicate in terms of esthetics.

摘要

背景/目的:在用于全瓷冠的陶瓷材料中,氧化锆具有高生物相容性和良好的机械性能,但其主要缺点包括低透明度和应力诱导相变。为了稳定高强度四方氧化锆多晶体(TZP),通常添加3 - 5摩尔%的氧化钇来制备氧化钇稳定的TZP(Y-TZP)。在本研究中,将三种商用Y-TZP陶瓷的光学性能与临床可用的二硅酸锂玻璃陶瓷材料的光学性能进行比较,并在体外分析透明度与晶体性能之间的关系。

材料与方法

从三种Y-TZP陶瓷和一块二硅酸锂制备了12个5毫米厚的标准化圆盘。使用带积分球的分光光度计测量绝对透明度。X射线衍射用于量化Y-TZP晶体的主要结构参数(即择优面、定量相和晶粒尺寸)。

结果

Y-TZP的产物主导相呈现四方晶格图案,择优面有微小变化。三种Y-TZP陶瓷的衍射图谱对透明度的影响较小,无显著差异(>0.05)。Y-TZP中54 - 70纳米的晶粒尺寸与透明度呈负相关。二硅酸锂试样的透明度明显高于三种Y-TZP试样(<0.001)。

结论

减小晶粒尺寸在开发高透明度Y-TZP陶瓷中起着至关重要的作用。三种Y-TZP陶瓷本质上是不透明的,但在美观方面比二硅酸锂的透明度更差。

https://cdn.ncbi.nlm.nih.gov/pmc/blobs/60ac/8403885/08743687a1ee/gr1.jpg

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