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含金属的紫外光固化木地板涂料的合成及其抗菌活性

Synthesis and Antibacterial Activity of Metal-Containing Ultraviolet-Cured Wood Floor Coatings.

作者信息

Chang Chia-Wei, Lu Kun-Tsung

机构信息

Department of Forestry, National Chung Hsing University, 250 Kuo-Kuang Rd., Taichung 402, Taiwan.

出版信息

Polymers (Basel). 2021 Sep 7;13(18):3022. doi: 10.3390/polym13183022.

DOI:10.3390/polym13183022
PMID:34577922
原文链接:https://pmc.ncbi.nlm.nih.gov/articles/PMC8469301/
Abstract

In our previous report, the antibacterial agents with different metals, mono(hydroxyethoxyethyl)phthalate [M(HEEP), M = Zn, Mn, and Ca], were synthesized. For increasing their yields, modified synthesis and purified processes were further investigated. The result of energy-dispersive X-ray spectroscopy showed the M(HEEP) could be stable and successfully synthesized, and their yields were raised to 73-85% from our previous report of 43-55%. For ultraviolet-cured wood floor coating application, the Zn(HEEP) was selected as an antibacterial agent and mixed with commercial UV wood floor coating. The effects on the antibacterial activity of UV films with different Zn(HEEP) additions of 0, 4, 8, and 12 phr as well as the commercial nano-Ag of 12 phr against were evaluated. In the static antibacterial test, the UV films with Zn(HEEP) additions had similar antibacterial activity of 57-59%. In another dynamic shaking antibacterial test, the film containing 12 phr Zn(HEEP) had the best antibacterial activity among all the UV films. On the film properties, the Zn(HEEP)-containing UV films had lower gloss and abrasion resistance, and slightly increased the hardness than those of UV film without Zn(HEEP) addition. However, there were no noticeable differences in mass retention, lightfastness, and thermal stability between UV films with and without the Zn(HEEP) addition. In this study, the 12 phr Zn(HEEP)-containing UV film provided the best antibacterial activity against and had the balanced film properties for application on the UV wood floor coating.

摘要

在我们之前的报告中，合成了含不同金属的抗菌剂单（羟基乙氧基乙基）邻苯二甲酸酯[M(HEEP)，M = Zn、Mn和Ca]。为提高其产率，进一步研究了改进的合成和纯化工艺。能量色散X射线光谱分析结果表明，M(HEEP)能够稳定合成，其产率从我们之前报告的43-55%提高到了73-85%。对于紫外光固化木地板涂料应用，选择Zn(HEEP)作为抗菌剂并与商用紫外光固化木地板涂料混合。评估了添加0、4、8和12 phr不同Zn(HEEP)以及添加12 phr商用纳米银的紫外光膜对[具体菌种未给出]的抗菌活性影响。在静态抗菌试验中，添加Zn(HEEP)的紫外光膜具有相似的57-59%的抗菌活性。在另一个动态振荡抗菌试验中，含12 phr Zn(HEEP)的膜在所有紫外光膜中具有最佳的抗菌活性。在膜性能方面，含Zn(HEEP)的紫外光膜光泽度和耐磨性较低，硬度比未添加Zn(HEEP)的紫外光膜略有增加。然而，添加和未添加Zn(HEEP)的紫外光膜在质量保留率、耐光性和热稳定性方面没有明显差异。在本研究中，含12 phr Zn(HEEP)的紫外光膜对[具体菌种未给出]具有最佳的抗菌活性，并且在紫外光固化木地板涂料应用中具有平衡的膜性能。

https://cdn.ncbi.nlm.nih.gov/pmc/blobs/f57b/8469301/574518222c30/polymers-13-03022-g009.jpg
https://cdn.ncbi.nlm.nih.gov/pmc/blobs/f57b/8469301/fd027efce57f/polymers-13-03022-g001.jpg
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https://cdn.ncbi.nlm.nih.gov/pmc/blobs/f57b/8469301/0cf73f1dfb31/polymers-13-03022-g006.jpg
https://cdn.ncbi.nlm.nih.gov/pmc/blobs/f57b/8469301/5b230ae6d391/polymers-13-03022-g007.jpg
https://cdn.ncbi.nlm.nih.gov/pmc/blobs/f57b/8469301/ecc04cd4c137/polymers-13-03022-g008.jpg
https://cdn.ncbi.nlm.nih.gov/pmc/blobs/f57b/8469301/574518222c30/polymers-13-03022-g009.jpg
https://cdn.ncbi.nlm.nih.gov/pmc/blobs/f57b/8469301/fd027efce57f/polymers-13-03022-g001.jpg
https://cdn.ncbi.nlm.nih.gov/pmc/blobs/f57b/8469301/f5e298168ee2/polymers-13-03022-g002.jpg
https://cdn.ncbi.nlm.nih.gov/pmc/blobs/f57b/8469301/2dd7f7130aad/polymers-13-03022-g003.jpg
https://cdn.ncbi.nlm.nih.gov/pmc/blobs/f57b/8469301/afbfb9eb8088/polymers-13-03022-g004.jpg
https://cdn.ncbi.nlm.nih.gov/pmc/blobs/f57b/8469301/00370a44658d/polymers-13-03022-g005.jpg
https://cdn.ncbi.nlm.nih.gov/pmc/blobs/f57b/8469301/0cf73f1dfb31/polymers-13-03022-g006.jpg
https://cdn.ncbi.nlm.nih.gov/pmc/blobs/f57b/8469301/5b230ae6d391/polymers-13-03022-g007.jpg
https://cdn.ncbi.nlm.nih.gov/pmc/blobs/f57b/8469301/ecc04cd4c137/polymers-13-03022-g008.jpg
https://cdn.ncbi.nlm.nih.gov/pmc/blobs/f57b/8469301/574518222c30/polymers-13-03022-g009.jpg

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