Jawaharram Gowtham Sriram, Barr Christopher M, Hattar Khalid, Dillon Shen J
Department of Materials Science and Engineering, University of Illinois Urbana-Champaign, Urbana, IL 61801, USA.
Sandia National Laboratories, P.O. Box 5800-1056, Albuquerque, NM 87185, USA.
Nanomaterials (Basel). 2021 Sep 18;11(9):2429. doi: 10.3390/nano11092429.
A series of nanopillar compression tests were performed on tungsten as a function of temperature using in situ transmission electron microscopy with localized laser heating. Surface oxidation was observed to form on the pillars and grow in thickness with increasing temperature. Deformation between 850 °C and 1120 °C is facilitated by long-range diffusional transport from the tungsten pillar onto adjacent regions of the YO-stabilized ZrO indenter. The constraint imposed by the surface oxidation is hypothesized to underly this mechanism for localized plasticity, which is generally the so-called whisker growth mechanism. The results are discussed in context of the tungsten fuzz growth mechanism in He plasma-facing environments. The two processes exhibit similar morphological features and the conditions under which fuzz evolves appear to satisfy the conditions necessary to induce whisker growth.
使用局部激光加热的原位透射电子显微镜,对钨进行了一系列纳米柱压缩试验,试验结果作为温度的函数呈现。观察到柱体表面形成氧化层,且随着温度升高,氧化层厚度增加。在850℃至1120℃之间,变形是由钨柱向钇稳定氧化锆压头相邻区域的长程扩散传输促成的。表面氧化所施加的约束被假定为这种局部塑性机制的基础,这通常就是所谓的晶须生长机制。结合面向氦等离子体环境中的钨模糊生长机制对结果进行了讨论。这两个过程表现出相似的形态特征,并且模糊发展的条件似乎满足诱导晶须生长所需的条件。