Liu Yan-Xing, Ke Zhi-Jiang, Li Run-Hua, Song Ju-Qing, Ruan Jing-Jing
Neutron Scattering Technical Engineering Research Center, School of Mechanical Engineering, Dongguan University of Technology, Dongguan 523808, China.
Guangdong-Hong Kong-Macao Joint Laboratory for Neutron Scattering Science and Technology, Dongguan University of Technology, Dongguan 523808, China.
Materials (Basel). 2021 Nov 16;14(22):6922. doi: 10.3390/ma14226922.
The grain growth behavior in a typical Ni-based superalloy was investigated using isothermal heat treatment experiments over a holding temperature range of 1353-1473 K. The experimental results showed that the grain structure continuously coarsened as the holding time and holding temperature increased during heat treatment. A classical parabolic grain growth model was used to explore the mechanism of grain growth under experimental conditions. The grain growth exponent was found to be slightly above 2. This indicates that the current grain growth in the studied superalloy is mainly governed by grain boundary migration with a minor pinning effect from the precipitates. Then, the grain growth in the studied superalloy during isothermal heat treatment was modelled by a cellular automaton (CA) with deterministic state switch rules. The microscale kinetics of grain growth is described by the correlation between the moving velocity and curvature of the grain boundary. The local grain boundary curvature is well evaluated by a template disk method. The grain boundary mobility was found to increase with increasing temperature. The relationship between the grain boundary mobility and temperature has been established. The developed CA model is capable of capturing the dependence of the grain size on the holding time under different holding temperatures.
通过在1353 - 1473 K的保温温度范围内进行等温热处理实验,研究了一种典型镍基高温合金中的晶粒生长行为。实验结果表明,在热处理过程中,随着保温时间和保温温度的增加,晶粒组织持续粗化。采用经典的抛物线晶粒生长模型来探究实验条件下的晶粒生长机制。发现晶粒生长指数略高于2。这表明在所研究的高温合金中,当前的晶粒生长主要由晶界迁移控制,析出相的钉扎作用较小。然后,用具有确定性状态切换规则的元胞自动机(CA)对所研究的高温合金在等温热处理过程中的晶粒生长进行建模。晶粒生长的微观动力学通过晶界移动速度和曲率之间的相关性来描述。采用模板圆盘法很好地评估了局部晶界曲率。发现晶界迁移率随温度升高而增加。建立了晶界迁移率与温度之间的关系。所开发的CA模型能够捕捉不同保温温度下晶粒尺寸对保温时间的依赖性。