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明胶在历史悠久的照片卷曲形成过程中的重要作用。

An Essential Role of Gelatin in the Formation Process of Curling in Long Historical Photos.

作者信息

Liu Jiaojiao, Li Yuhu, Hu Daodao, Chao Xiaolian, Zhou Yajun, Wang Juanli

机构信息

Engineering Research Center of Historical Cultural Heritage Conservation, Ministry of Education, School of Materials Science and Engineering, Shaanxi Normal University, Xi'an 710119, China.

出版信息

Polymers (Basel). 2021 Nov 11;13(22):3894. doi: 10.3390/polym13223894.

DOI:10.3390/polym13223894
PMID:34833193
原文链接:https://pmc.ncbi.nlm.nih.gov/articles/PMC8622965/
Abstract

Curling disease in long historical photos significantly affects the presentation of cultural heritage information. However, people lack attention to the formation process and microstructural changes of photo curling. In this article, a long historical photo (1912-1949 AD) collected by the Second Historical Archives of China was taken as the research object, and the formation process and cause of the curling were further explored. Firstly, Fourier-transform infrared spectroscopy (FTIR), X-ray diffraction (XRD), scanning electron microscope (SEM), X-ray energy disperse spectrometer (EDS), and other instruments were used to analyze the material composition of the long historical photo. It was found that the photographic paper was made of gelatin, barium sulfate, and plant fiber layers. Then, the effects of hygrothermal environments on curling and contraction in the gelatin layer and simulated photographic paper were explored. Meanwhile, the formation process and main influence factors of the curling were preliminarily revealed. The morphological analysis by SEM was carried out to identify the inner correlation between the microstructure and curling of photos. Finally, the possible formation cause of photo curling was analyzed. This study provides a scientific basis and experimental data for the preservation and restoration of long historical photos based on gelatin.

摘要

历史久远照片中的卷曲现象严重影响文化遗产信息的呈现。然而，人们对照片卷曲的形成过程和微观结构变化缺乏关注。本文以中国第二历史档案馆收藏的一张历史久远的照片（公元1912 - 1949年）为研究对象，进一步探究其卷曲的形成过程及原因。首先，利用傅里叶变换红外光谱仪（FTIR）、X射线衍射仪（XRD）、扫描电子显微镜（SEM）、X射线能谱仪（EDS）等仪器分析了这张历史久远照片的材料成分。发现相纸由明胶、硫酸钡和植物纤维层组成。然后，探究了湿热环境对明胶层及模拟相纸卷曲和收缩的影响。同时，初步揭示了卷曲的形成过程及主要影响因素。通过扫描电子显微镜进行形态分析，以确定照片微观结构与卷曲之间的内在关联。最后，分析了照片卷曲可能的形成原因。本研究为基于明胶的历史久远照片的保存与修复提供了科学依据和实验数据。

https://cdn.ncbi.nlm.nih.gov/pmc/blobs/461b/8622965/5d1467d46348/polymers-13-03894-g007.jpg
https://cdn.ncbi.nlm.nih.gov/pmc/blobs/461b/8622965/e0be6dc7cda3/polymers-13-03894-g001.jpg
https://cdn.ncbi.nlm.nih.gov/pmc/blobs/461b/8622965/b5aeb7dcf4c1/polymers-13-03894-g002.jpg
https://cdn.ncbi.nlm.nih.gov/pmc/blobs/461b/8622965/f62a830a6533/polymers-13-03894-g003.jpg
https://cdn.ncbi.nlm.nih.gov/pmc/blobs/461b/8622965/66a6cc850638/polymers-13-03894-g004.jpg
https://cdn.ncbi.nlm.nih.gov/pmc/blobs/461b/8622965/4d5ef053b50d/polymers-13-03894-g005.jpg
https://cdn.ncbi.nlm.nih.gov/pmc/blobs/461b/8622965/4d177bab0938/polymers-13-03894-g006.jpg
https://cdn.ncbi.nlm.nih.gov/pmc/blobs/461b/8622965/5d1467d46348/polymers-13-03894-g007.jpg
https://cdn.ncbi.nlm.nih.gov/pmc/blobs/461b/8622965/e0be6dc7cda3/polymers-13-03894-g001.jpg
https://cdn.ncbi.nlm.nih.gov/pmc/blobs/461b/8622965/b5aeb7dcf4c1/polymers-13-03894-g002.jpg
https://cdn.ncbi.nlm.nih.gov/pmc/blobs/461b/8622965/f62a830a6533/polymers-13-03894-g003.jpg
https://cdn.ncbi.nlm.nih.gov/pmc/blobs/461b/8622965/66a6cc850638/polymers-13-03894-g004.jpg
https://cdn.ncbi.nlm.nih.gov/pmc/blobs/461b/8622965/4d5ef053b50d/polymers-13-03894-g005.jpg
https://cdn.ncbi.nlm.nih.gov/pmc/blobs/461b/8622965/4d177bab0938/polymers-13-03894-g006.jpg
https://cdn.ncbi.nlm.nih.gov/pmc/blobs/461b/8622965/5d1467d46348/polymers-13-03894-g007.jpg

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