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韭菜提取物复合纤维素薄膜的制备与表征

Preparation and Characterization of Chinese Leek Extract Incorporated Cellulose Composite Films.

作者信息

Zeng Qiying, Xiao Naiyu, Zhang Xueqin, Luo Wenhan, Xiao Gengshen, Zhai Wanjing, Zhong Le, Lan Bifeng

机构信息

College of Light Industry and Food Science, Zhongkai University of Agriculture and Engineering, Guangzhou, China.

Guangzhou Furui High Energy Technology Co., Ltd, Guangzhou, China.

出版信息

Front Bioeng Biotechnol. 2021 Nov 15;9:731749. doi: 10.3389/fbioe.2021.731749. eCollection 2021.

Abstract

This study aimed to prepare microcrystalline cellulose (MCC) films with good mechanical properties plasticization using a Chinese leek (CL, ) extract. The microstructure, crystal structure, mechanical properties, barrier ability, and thermal properties of the films were investigated. The chemical structure analysis of CL extract showed the existence of cellulose, lignin, and low-molecular-weight substances, such as polysaccharides, pectins, and waxes, which could act as plasticizers to enhance the properties of MCC:CL biocomposite films. The results of scanning electron microscopy and atomic force microscopy analyses indicated the good compatibility between MCC and CL extract. When the volume ratio of MCC:CL was 7:3, the MCC:CL biocomposite film exhibited the best comprehensive performance in terms of water vapor permeability (2.11 × 10 g/m·s·Pa), elongation at break (13.2 ± 1.8%), and tensile strength (24.7 ± 2.5 MPa). The results of a UV absorption analysis demonstrated that the addition of CL extract improved the UV-shielding performance of the films. Therefore, this work not only proposes a facile method to prepare MCC films with excellent mechanical properties plasticization using CL extract but also broadens the potential applications of MCC films in the packaging area.

摘要

本研究旨在使用韭菜(CL)提取物制备具有良好机械性能的微晶纤维素(MCC)增塑薄膜。对薄膜的微观结构、晶体结构、机械性能、阻隔性能和热性能进行了研究。CL提取物的化学结构分析表明,其中存在纤维素、木质素以及多糖、果胶和蜡等低分子量物质,这些物质可作为增塑剂来增强MCC:CL生物复合薄膜的性能。扫描电子显微镜和原子力显微镜分析结果表明MCC与CL提取物之间具有良好的相容性。当MCC:CL的体积比为7:3时,MCC:CL生物复合薄膜在水蒸气透过率(2.11×10⁻⁶g/m·s·Pa)、断裂伸长率(13.2±1.8%)和拉伸强度(24.7±2.5MPa)方面表现出最佳的综合性能。紫外线吸收分析结果表明,CL提取物的添加提高了薄膜的紫外线屏蔽性能。因此,这项工作不仅提出了一种使用CL提取物制备具有优异机械性能的增塑MCC薄膜的简便方法,还拓宽了MCC薄膜在包装领域的潜在应用。

https://cdn.ncbi.nlm.nih.gov/pmc/blobs/8c49/8634590/5a87d22d6169/fbioe-09-731749-g010.jpg

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