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美国国家标准与技术研究院纳米量热计的设计、制造与校准实用指南。

Practical Guide to the Design, Fabrication, and Calibration of NIST Nanocalorimeters.

作者信息

Yi Feng, Grapes Michael D, LaVan David A

机构信息

National Institute of Standards and Technology, Gaithersburg, MD 20899, USA.

Lawrence Livermore National Laboratory, Livermore, CA 94550, USA.

出版信息

J Res Natl Inst Stand Technol. 2019 Dec 16;124:1-19. doi: 10.6028/jres.124.021. eCollection 2019.

DOI:10.6028/jres.124.021
PMID:34877173
原文链接:https://pmc.ncbi.nlm.nih.gov/articles/PMC7340549/
Abstract

We report here on the design, fabrication, and calibration of nanocalorimeter sensors used in the National Institute of Standards and Technology (NIST) Nanocalorimetry Measurements Project. These small-scale thermal analysis instruments are produced using silicon microfabrication approaches. A single platinum line serves as both the heater and temperature sensor, and it is made from a 500 μm wide, 100 nm thick platinum trace, suspended on a 100 nm thick silicon nitride membrane for thermal isolation. Supplemental materials to this article (available online) include drawing files and LabVIEW code used in the fabrication and calibration process.

摘要

我们在此报告美国国家标准与技术研究院(NIST)纳米量热法测量项目中使用的纳米量热传感器的设计、制造和校准情况。这些小型热分析仪器采用硅微加工方法制造。一条铂线同时用作加热器和温度传感器,它由一条宽500μm、厚100nm的铂迹线制成,悬浮在100nm厚的氮化硅膜上以实现热隔离。本文的补充材料(可在线获取)包括制造和校准过程中使用的绘图文件和LabVIEW代码。

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本文引用的文献

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Multi-environment Nanocalorimeter with Electrical Contacts for Use in the Scanning Electron Microscope.用于扫描电子显微镜的带电接触的多环境纳米量热仪。
Mater Horiz. 2017 Nov;4(6):1128-1134. doi: 10.1039/C7MH00513J. Epub 2017 Sep 11.
2
Microhotplate Temperature Sensor Calibration and BIST.微热板温度传感器校准与内建自测试
J Res Natl Inst Stand Technol. 2011 Dec 11;116(6):827-38. doi: 10.6028/jres.116.025. Print 2011 Nov-Dec.
3
Nanocalorimetry-coupled time-of-flight mass spectrometry: identifying evolved species during high-rate thermal measurements.纳米量热法与飞行时间质谱联用:在高速热测量过程中识别逸出物种。
Anal Chem. 2015 Oct 6;87(19):9740-4. doi: 10.1021/acs.analchem.5b01872.
4
Hydrated/dehydrated lipid phase transitions measured using nanocalorimetry.使用纳米量热法测量水合/脱水脂质相转变。
J Pharm Sci. 2014 Nov;103(11):3442-3447. doi: 10.1002/jps.24187. Epub 2014 Sep 24.
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Combining nanocalorimetry and dynamic transmission electron microscopy for in situ characterization of materials processes under rapid heating and cooling.结合纳米量热法和动态透射电子显微镜对快速加热和冷却过程中的材料过程进行原位表征。
Rev Sci Instrum. 2014 Aug;85(8):084902. doi: 10.1063/1.4892537.
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A novel on-chip three-dimensional micromachined calorimeter with fully enclosed and suspended thin-film chamber for thermal characterization of liquid samples.一种新型片上三维微加工量热计,具有全封闭和悬浮的薄膜腔,用于液体样品的热特性分析。
Biomicrofluidics. 2014 May 8;8(3):034101. doi: 10.1063/1.4875656. eCollection 2014 May.
7
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J Am Chem Soc. 2013 Sep 25;135(38):14286-98. doi: 10.1021/ja4059958. Epub 2013 Sep 12.
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Synthesis and characterization of single-layer silver-decanethiolate lamellar crystals.单层银-十一硫醇层状晶体的合成与表征。
J Am Chem Soc. 2011 Mar 30;133(12):4367-76. doi: 10.1021/ja107817x. Epub 2011 Mar 3.
9
Thin film nanocalorimeter for heat capacity measurements of 30 nm films.用于测量30纳米薄膜热容的薄膜纳米量热计。
Rev Sci Instrum. 2009 Jun;80(6):063901. doi: 10.1063/1.3142463.
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