Lu Zhaofeng, Kong Lin, He Zhaoyi, Xu Hao, Yang Kang, Shen Zuzhen, Huang Zhaodong
School of Mechanotronics and Vehicle Engineering, Chongqing Jiaotong University, Chongqing 400074, China.
School of Civil Engineering, Chongqing Jiaotong University, Chongqing 400074, China.
Materials (Basel). 2021 Nov 30;14(23):7363. doi: 10.3390/ma14237363.
In order to solve the problems of the smooth surface of basalt fiber and its weak interfacial adhesion with emulsified asphalt cold recycled mixture, a silane coupling agent (KH550) was used to treat the surface of basalt fiber and the effects of treatment concentration and soaking time on fiber modification were studied. The influence of silane coupling-modified basalt fiber (MBF) on the rheological properties of emulsified asphalt evaporation residue was studied at high and low temperatures using three routine index tests: a dynamic shear rheological test (DSR), a bending beam rheological test (BBR), and a force ductility test. The elemental changes of the fiber before and after modification and the microstructure of the emulsified asphalt evaporation residue with the coupling-modified fiber were analyzed by Fourier infrared spectroscopy (FT-IR), scanning electron microscopy (SEM), and X-ray energy dispersive spectroscopy (EDS), which is used to study the modification mechanism of emulsified asphalt evaporation residue reinforced by coupling-modified fiber. The results indicate that the concentration and soaking time of the silane coupling agent have a great influence on the surface morphology and mechanical properties of the fiber, and that the optimal treatment concentration is 1.0% and the optimal soaking time is 60 min. The addition of coupling-modified fibers can reduce the phase angle and unrecoverable creep compliance of emulsified asphalt evaporation residue, increase the rutting factor and creep recovery rate, and improve the elastic recovery ability and permanent deformation resistance. However, excessive fiber will weaken the ductility of emulsified asphalt at low temperatures. The appropriate content of silane coupling-modified fiber (MBF) is 1.5%. After silane coupling modification, the fiber surface becomes rough and cohesion is enhanced between the fiber and the emulsified asphalt base. Silane coupling-modified basalt fiber (MBF) acts as reinforcement for stability and bridging cracks.
为了解决玄武岩纤维表面光滑及其与乳化沥青冷再生混合料界面粘结力弱的问题,采用硅烷偶联剂(KH550)对玄武岩纤维表面进行处理,并研究处理浓度和浸泡时间对纤维改性的影响。通过动态剪切流变试验(DSR)、弯曲梁流变试验(BBR)和强制延度试验这三项常规指标试验,研究了硅烷偶联改性玄武岩纤维(MBF)在高温和低温下对乳化沥青蒸发残留物流变性能的影响。利用傅里叶红外光谱(FT-IR)、扫描电子显微镜(SEM)和X射线能谱仪(EDS)分析了改性前后纤维的元素变化以及含偶联改性纤维的乳化沥青蒸发残留物的微观结构,以此研究偶联改性纤维增强乳化沥青蒸发残留物的改性机理。结果表明,硅烷偶联剂的浓度和浸泡时间对纤维的表面形态和力学性能有很大影响,最佳处理浓度为1.0%,最佳浸泡时间为60min。偶联改性纤维的加入可降低乳化沥青蒸发残留物的相位角和不可恢复蠕变柔量,提高车辙因子和蠕变恢复率,改善弹性恢复能力和抗永久变形能力。然而,纤维过多会削弱乳化沥青在低温下的延度。硅烷偶联改性纤维(MBF)的适宜含量为1.5%。经过硅烷偶联改性后,纤维表面变得粗糙,纤维与乳化沥青基体之间的粘结力增强。硅烷偶联改性玄武岩纤维(MBF)起到增强稳定性和桥接裂缝的作用。