Léveillé Cyril, Desjardins Kewin, Popescu Horia, Vondungbo Boris, Hennes Marcel, Delaunay Renaud, Jal Emmanuelle, De Angelis Dario, Pancaldi Matteo, Pedersoli Emanuele, Capotondi Flavio, Jaouen Nicolas
Synchrotron SOLEIL, L'Orme des Merisiers, Saint-Aubin, BP48, 91192 Gif-sur-Yvette, France.
Sorbonne Université, CNRS, Laboratoire de Chimie Physique-Matière et Rayonnement, LCPMR, 75005 Paris, France.
J Synchrotron Radiat. 2022 Jan 1;29(Pt 1):103-110. doi: 10.1107/S1600577521012303.
The latest Complementary Metal Oxide Semiconductor (CMOS) 2D sensors now rival the performance of state-of-the-art photon detectors for optical application, combining a high-frame-rate speed with a wide dynamic range. While the advent of high-repetition-rate hard X-ray free-electron lasers (FELs) has boosted the development of complex large-area fast CCD detectors in the extreme ultraviolet (EUV) and soft X-ray domains, scientists lacked such high-performance 2D detectors, principally due to the very poor efficiency limited by the sensor processing. Recently, a new generation of large back-side-illuminated scientific CMOS sensors (CMOS-BSI) has been developed and commercialized. One of these cost-efficient and competitive sensors, the GSENSE400BSI, has been implemented and characterized, and the proof of concept has been carried out at a synchrotron or laser-based X-ray source. In this article, we explore the feasibility of single-shot ultra-fast experiments at FEL sources operating in the EUV/soft X-ray regime with an AXIS-SXR camera equipped with the GSENSE400BSI-TVISB sensor. We illustrate the detector capabilities by performing a soft X-ray magnetic scattering experiment at the DiProi end-station of the FERMI FEL. These measurements show the possibility of integrating this camera for collecting single-shot images at the 50 Hz operation mode of FERMI with a cropped image size of 700 × 700 pixels. The efficiency of the sensor at a working photon energy of 58 eV and the linearity over the large FEL intensity have been verified. Moreover, on-the-fly time-resolved single-shot X-ray resonant magnetic scattering imaging from prototype Co/Pt multilayer films has been carried out with a time collection gain of 30 compared to the classical start-and-stop acquisition method performed with the conventional CCD-BSI detector available at the end-station.
最新的互补金属氧化物半导体(CMOS)二维传感器现在在光学应用方面可与最先进的光子探测器相媲美,它结合了高帧率速度和宽动态范围。虽然高重复率硬X射线自由电子激光(FEL)的出现推动了极紫外(EUV)和软X射线领域复杂大面积快速电荷耦合器件(CCD)探测器的发展,但科学家们缺乏这种高性能二维探测器,主要原因是传感器处理导致效率极低。最近,新一代大面积背照式科学CMOS传感器(CMOS-BSI)已被开发并商业化。其中一种具有成本效益且竞争力强的传感器GSENSE400BSI已被应用并进行了特性表征,其概念验证已在基于同步加速器或激光的X射线源上完成。在本文中,我们探讨了使用配备GSENSE400BSI-TVISB传感器的AXIS-SXR相机在EUV/软X射线波段运行的FEL源上进行单次超快实验的可行性。我们通过在FERMI FEL的DiProi终端站进行软X射线磁散射实验来说明探测器的能力。这些测量结果表明,有可能将该相机集成到FERMI的50Hz运行模式下,以采集裁剪后图像尺寸为700×700像素的单次图像。已验证了该传感器在58eV工作光子能量下的效率以及在大FEL强度范围内的线性度。此外,与终端站现有的传统CCD-BSI探测器采用的经典启停采集方法相比,已对原型Co/Pt多层膜进行了实时时间分辨单次X射线共振磁散射成像,时间采集增益为30。