Desjardins Kewin, Medjoubi Kadda, Sacchi Maurizio, Popescu Horia, Gaudemer Roland, Belkhou Rachid, Stanescu Stefan, Swaraj Sufal, Besson Adrien, Vijayakumar Jaianth, Pautard Stéphanie, Noureddine Arafat, Mercère Pascal, Da Silva Paulo, Orsini Fabienne, Menneglier Claude, Jaouen Nicolas
Synchrotron SOLEIL, Saint-Aubin, Gif-sur-Yvette, 91192, France.
J Synchrotron Radiat. 2020 Nov 1;27(Pt 6):1577-1589. doi: 10.1107/S160057752001262X. Epub 2020 Oct 26.
The impressive progress in the performance of synchrotron radiation sources is nowadays driven by the so-called `ultimate storage ring' projects which promise an unprecedented improvement in brightness. Progress on the detector side has not always been at the same pace, especially as far as soft X-ray 2D detectors are concerned. While the most commonly used detectors are still based on microchannel plates or CCD technology, recent developments of CMOS (complementary metal oxide semiconductor)-type detectors will play an ever more important role as 2D detectors in the soft X-ray range. This paper describes the capabilities and performance of a camera equipped with a newly commercialized backside-illuminated scientific CMOS (sCMOS-BSI) sensor, integrated in a vacuum environment, for soft X-ray experiments at synchrotron sources. The 4 Mpixel sensor reaches a frame rate of up to 48 frames s while matching the requirements for X-ray experiments in terms of high-intensity linearity (>98%), good spatial homogeneity (<1%), high charge capacity (up to 80 ke), and low readout noise (down to 2 e r.m.s.) and dark current (3 e per second per pixel). Performance evaluations in the soft X-ray range have been carried out at the METROLOGIE beamline of the SOLEIL synchrotron. The quantum efficiency, spatial resolution (24 line-pairs mm), energy resolution (<100 eV) and radiation damage versus the X-ray dose (<600 Gy) have been measured in the energy range from 40 to 2000 eV. In order to illustrate the capabilities of this new sCMOS-BSI sensor, several experiments have been performed at the SEXTANTS and HERMES soft X-ray beamlines of the SOLEIL synchrotron: acquisition of a coherent diffraction pattern from a pinhole at 186 eV, a scattering experiment from a nanostructured Co/Cu multilayer at 767 eV and ptychographic imaging in transmission at 706 eV.
如今,同步辐射源性能方面令人瞩目的进展是由所谓的“终极储存环”项目推动的,这些项目有望在亮度上实现前所未有的提升。探测器方面的进展并非总是同步的,尤其是在软X射线二维探测器方面。虽然最常用的探测器仍基于微通道板或电荷耦合器件(CCD)技术,但互补金属氧化物半导体(CMOS)型探测器的最新发展将在软X射线范围内作为二维探测器发挥越来越重要的作用。本文描述了一款配备新商业化的背照式科学互补金属氧化物半导体(sCMOS-BSI)传感器、集成于真空环境中的相机,用于同步辐射源的软X射线实验的能力和性能。这款400万像素的传感器在满足X射线实验对高强度线性度(>98%)、良好空间均匀性(<1%)、高电荷容量(高达80ke)、低读出噪声(低至2e均方根)和暗电流(每秒每像素3e)要求的同时,帧率可达每秒48帧。在SOLEIL同步辐射装置的计量学光束线上进行了软X射线范围内的性能评估。在40至2000eV的能量范围内测量了量子效率、空间分辨率(每毫米24线对)、能量分辨率(<100eV)以及辐射损伤与X射线剂量(<600Gy)的关系。为了说明这款新型sCMOS-BSI传感器的能力,在SOLEIL同步辐射装置的SEXTANTS和HERMES软X射线光束线上进行了多项实验:在186eV下采集针孔的相干衍射图案、在767eV下对纳米结构的Co/Cu多层膜进行散射实验以及在706eV下进行透射式叠层成像。