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奥氏体钢表面电化学法制备的多孔层的制备与性能

Production and Properties of the Porous Layer Obtained by the Electrochemical Method on the Surface of Austenitic Steel.

作者信息

Ossowska Agnieszka, Ryl Jacek, Sternicki Tomasz

机构信息

Faculty of Mechanical Engineering and Ship Technology, Gdansk University of Technology, 80-233 Gdańsk, Poland.

Advanced Materials Center, Faculty of Applied Physics and Mathematics, Gdansk University of Technology, 80-233 Gdańsk, Poland.

出版信息

Materials (Basel). 2022 Jan 26;15(3):949. doi: 10.3390/ma15030949.

Abstract

The growing demand for implants has seen increasing interest in the introduction of new technologies and surface modification methods of metal biomaterials. This research aimed to produce and characterize a porous layer grown on austenitic stainless steel 316L, obtained via the anodization process near the micro-arc oxidation, i.e., low voltage micro-arc oxidation (LVMAO). The discussed layer significantly influences the properties of metallic biomedical materials. The surface topography, layer thickness, surface roughness, pore diameter, elemental composition, crystal structure, and surface wettability were assessed for all anodized layers, together with the resultant corrosion resistance. Attention was paid to the influence of the process parameters that affect the specification of the produced layer. The obtained results showed surface development and different sized pores in the modified layers, as well as an increase in corrosion resistance in the Ringer's solution.

摘要

对植入物需求的不断增长,使得人们对金属生物材料新技术的引入和表面改性方法越来越感兴趣。本研究旨在制备并表征在奥氏体不锈钢316L上生长的多孔层,该多孔层通过微弧氧化附近的阳极氧化工艺获得,即低压微弧氧化(LVMAO)。所讨论的层对金属生物医学材料的性能有显著影响。对所有阳极氧化层的表面形貌、层厚度、表面粗糙度、孔径、元素组成、晶体结构和表面润湿性进行了评估,并测定了其耐腐蚀性。研究关注了影响所制备层规格的工艺参数的影响。所得结果表明,改性层表面有明显变化且存在不同尺寸的孔隙,同时在林格氏溶液中的耐腐蚀性有所提高。

https://cdn.ncbi.nlm.nih.gov/pmc/blobs/48c3/8837965/e964e17c1770/materials-15-00949-g001.jpg

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