Wołowiec-Korecka Emilia, Czepułkowska-Pawlak Weronika, Kula Zofia, Klimek Leszek
Institute of Materials Science and Engineering, Faculty of Mechanical Engineering, Lodz University of Technology, B. Stefanowskiego 1/15, 90-537 Lodz, Poland.
Department of Dental Technology, Medical University of Lodz, Pomorska 251, 92-213 Lodz, Poland.
Materials (Basel). 2022 Jan 26;15(3):964. doi: 10.3390/ma15030964.
The SiC abrasive blasting parameters are vital in ensuring a suitable bond between dental ceramics and the Ni-Cr alloy. The purpose of this in vitro test was to examine the strength of the joint between the Ni-Cr alloy and fused dental ceramics for SiC abrasive blasting at a specific pressure (400, 600 kPa) and particle size (50, 110, 250 µm) in order to determine the optimal treatment parameters. The test also accounted for thermal loads (5000 cycles, 5-55 °C) to which the metal-ceramic joint is subjected during use. One hundred and forty-four Ni-Cr cylinders were divided into six groups ( = 12) and subjected to the airborne-particle abrasion with SiC with various pressure and grit size parameters. After treatment, the specimens were rinsed, dried, fused to dental ceramics, and examined for their shear strength using the Zwick/Roell Z020 machine. The results were statistically analysed using the ANOVA analysis of variance (α = 0.05). The highest metal-ceramic joint strength was obtained for abrasive blasting with 110 and 250 µm SiC grit at a pressure of 400 kPa. This relationship was also observed after the joint was subjected to thermal loads (5000 thermocycles). Additionally, thermal loads did not significantly reduce the joint's strength compared with non-loaded joints. For small SiC abrasive grit sizes (50 µm) under pressure 400 kPa, the treatment pressure had a significant effect on the strength of the joint ( < 0.05). For larger particle sizes, the pressure had no effect. After abrasive blasting using SiC, the Ni-Cr metal-ceramic joint retained its properties, even under thermal load, ensuring the joint properties' stability during use.
碳化硅喷砂参数对于确保牙科陶瓷与镍铬合金之间形成合适的结合至关重要。这项体外测试的目的是,在特定压力(400、600千帕)和颗粒尺寸(50、110、250微米)下,检测镍铬合金与烤瓷牙之间结合的强度,以确定最佳处理参数。该测试还考虑了金属陶瓷结合在使用过程中所承受的热负荷(5000次循环,5 - 55摄氏度)。144个镍铬圆柱体被分为六组(每组 = 12个),并使用不同压力和粒度参数的碳化硅进行空气颗粒磨损处理。处理后,对样本进行冲洗、干燥,与牙科陶瓷熔合,然后使用Zwick/Roell Z020机器检测其剪切强度。使用方差分析(α = 0.05)对结果进行统计分析。在400千帕压力下,使用110微米和250微米碳化硅砂粒进行喷砂处理时,获得了最高的金属陶瓷结合强度。在结合承受热负荷(5000次热循环)后,也观察到了这种关系。此外,与未加载的结合相比,热负荷并未显著降低结合的强度。对于400千帕压力下的小尺寸碳化硅磨料粒度(50微米),处理压力对结合强度有显著影响(< 0.05)。对于较大的颗粒尺寸,压力没有影响。使用碳化硅进行喷砂处理后,镍铬金属陶瓷结合即使在热负荷下仍能保持其性能,确保了使用过程中结合性能的稳定性。