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镍铬合金表面喷砂处理对其与液态陶瓷润湿性的影响。

Effect of Ni-Cr Alloy Surface Abrasive Blasting on Its Wettability by Liquid Ceramics.

作者信息

Czepułkowska-Pawlak Weronika, Klimek Leszek, Makówka Marcin, Wołowiec-Korecka Emilia

机构信息

Institute of Materials Science and Engineering, Faculty of Mechanical Engineering, Lodz University of Technology, Stefanowskiego 1/15, 90-924 Łódź, Poland.

出版信息

Materials (Basel). 2021 Apr 16;14(8):2007. doi: 10.3390/ma14082007.

Abstract

An adequate surface is essential in ensuring a solid bond between the metal and dental ceramics for metal framework wettability. This work is aimed at investigating the effect of variable abrasive blasting parameters on Ni-Cr alloy surface's ability to be wetted with liquid ceramics at elevated temperatures. One-hundred and sixty-eight samples were divided into 12 groups ( = 14), which were sandblasted using variable parameters: type of abrasive (AlO and SiC), the grain size of the abrasive (50, 110, and 250 µm), and processing pressure (400 and 600 kPa). After treatment, the samples were cleaned in an ultrasonic cleaner and dried under compressed air. Dental ceramics were applied to the prepared surfaces via drops, and the wettability was tested in a vacuum oven at temperatures in the range of 850-1000 °C. The results were statistically analyzed using ANOVA (α = 0.05). For all surfaces, the contact angles were less than 90° at temperatures below 875 °C. For AlO, the best wettability was observed for the smallest particles and, for SiC, the largest particles. The ability to wet the surface of a Ni-Cr alloy is related to its sandblasting properties, such as roughness or the percentage of embedded abrasive particles. It should not be the only factor determining the selection of abrasive blasting parameters when creating a prosthetic restoration.

摘要

对于金属框架的润湿性而言,足够的表面对于确保金属与牙科陶瓷之间形成牢固的结合至关重要。这项工作旨在研究可变喷砂参数对镍铬合金表面在高温下被液态陶瓷润湿能力的影响。168个样品被分为12组(每组n = 14),使用可变参数进行喷砂处理:磨料类型(Al₂O₃和SiC)、磨料粒度(50、110和250 µm)以及加工压力(400和600 kPa)。处理后,样品在超声波清洗器中清洗并在压缩空气下干燥。通过滴加的方式将牙科陶瓷施加到制备好的表面上,并在850 - 1000 °C的温度范围内在真空炉中测试润湿性。使用方差分析(α = 0.05)对结果进行统计学分析。对于所有表面,在温度低于875 °C时接触角均小于90°。对于Al₂O₃,最小颗粒表现出最佳润湿性,而对于SiC,最大颗粒表现出最佳润湿性。镍铬合金表面的润湿能力与其喷砂特性有关,如粗糙度或嵌入磨料颗粒的百分比。在制作修复体时,它不应是决定喷砂参数选择的唯一因素。

https://cdn.ncbi.nlm.nih.gov/pmc/blobs/7102/8073811/02835b701312/materials-14-02007-g001.jpg

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