Aghris S, Alaoui O Tahiri, Laghrib F, Farahi A, Bakasse M, Saqrane S, Lahrich S, El Mhammedi M A
Sultan Moulay Slimane University, Laboratory of Materials Science, Mathematics and Environment, Polydisciplinary Faculty, Khouribga, Morocco.
Moulay Ismail University, Laboratory of Physical Chemistry, Materials and Environment, Sciences and Technologies Faculty, Errachidia, Morocco.
Curr Res Food Sci. 2022 Feb 14;5:401-413. doi: 10.1016/j.crfs.2022.02.005. eCollection 2022.
Flubendiamide (FBD) is the first commercially available phthalic acid diamide that targets ryanodine receptors (RyRs) in insects, which play a major role in lepidoptera control. However, excessive use of FBD can influence the quality of treated products leading to toxic effects on human health. The availability of rapid and convenient methods for evaluating FBD amount in the environment is necessary. Therefore, analytical methods were developed for the determination of residues of FBD and its metabolite desiodo in different food matrices like tomato, cabbage, pigeon pea, apple, chilli and rice. The current review carries forward methods for FBD residues analysis in foods by using several chromatographic techniques including sample preparation steps. The comparison between the different methods employed for quantitative and qualitative analysis of food quality and safety is also discussed. Liquid chromatography (LC) is the predominant analytical method for assessing the quality of foods treated with FBD. Studies related to LC coupled multichannel detector (Ultraviolet (UV), Mass spectrometry (MS)) are also applied to detect pesticide residues. Extraction and clean up steps are essential to obtain reliable results. Moreover, this review reports the allowed limits of residues for the safety of consuming products treated with FBD.
氟苯虫酰胺（FBD）是第一种上市的邻苯二甲酸二酰胺类杀虫剂，作用于昆虫的兰尼碱受体（RyRs），在鳞翅目害虫防治中发挥重要作用。然而，过度使用氟苯虫酰胺会影响处理后产品的质量，对人体健康产生毒性作用。因此，需要快速便捷的方法来评估环境中氟苯虫酰胺的含量。为此，开发了分析方法用于测定不同食品基质（如番茄、卷心菜、木豆、苹果、辣椒和大米）中氟苯虫酰胺及其代谢物去碘氟苯虫酰胺的残留量。本综述介绍了使用多种色谱技术（包括样品制备步骤）分析食品中氟苯虫酰胺残留量的方法。还讨论了用于食品质量和安全定量与定性分析的不同方法之间的比较。液相色谱（LC）是评估经氟苯虫酰胺处理食品质量的主要分析方法。与液相色谱联用多通道检测器（紫外（UV）、质谱（MS））相关的研究也用于检测农药残留。提取和净化步骤对于获得可靠结果至关重要。此外，本综述报告了食用经氟苯虫酰胺处理产品安全所需的残留限量。
