Al-Dalali Sam, Li Cong, Xu Baocai
School of Food and Biological Engineering, Hefei University of Technology, Hefei 230601, China; China Light Industry Key Laboratory of Meat Microbial Control and Utilization, Hefei University of Technology, Hefei 230009, China; Department of Food Science and Technology, Faculty of Agriculture and Food Science, Ibb University, Ibb 70270, Yemen.
School of Food and Biological Engineering, Hefei University of Technology, Hefei 230601, China; China Light Industry Key Laboratory of Meat Microbial Control and Utilization, Hefei University of Technology, Hefei 230009, China.
Food Chem. 2022 Aug 15;385:132629. doi: 10.1016/j.foodchem.2022.132629. Epub 2022 Mar 4.
This study aimed to evaluate the effect of frozen storage on the changes in volatile aldehydes (VAs), volatile alcohols (VCs), lipid oxidation, and fatty acid composition of marinated roasted beef meat. Thirty VAs and VCs were identified in all meat samples by using headspace solid-phase microextraction-gas chromatography-mass spectrometry. The total concentrations of VAs increased with storage periods up to four months and gradually decreased. Whereas the total concentrations of VCs decreased with prolonged storage periods. The contents of thiobarbituric acid reactive substances and hexanal increased with prolonged storage periods in all samples until four months and then gradually decreased except the hexanal contents in the control sample (BS1), which showed an increase up to six months. Saturated and monounsaturated fatty acids decreased after storage in all samples except the control. By contrast, polyunsaturated fatty acids increased with prolonged storage in all samples. The correlation analysis showed the positive correlation of flavor compounds with fatty acids, E-nose, and sensory notes.
本研究旨在评估冷冻储存对腌制烤牛肉中挥发性醛类(VAs)、挥发性醇类(VCs)、脂质氧化及脂肪酸组成变化的影响。通过顶空固相微萃取-气相色谱-质谱联用技术,在所有肉样中鉴定出30种挥发性醛类和挥发性醇类。挥发性醛类的总浓度在储存期长达四个月时随时间增加,之后逐渐下降。而挥发性醇类的总浓度则随储存期延长而降低。所有样品中硫代巴比妥酸反应物和己醛的含量在储存期长达四个月时随时间增加,之后逐渐下降,但对照样品(BS1)中的己醛含量除外,其在长达六个月的时间里持续增加。除对照样品外,所有样品储存后饱和脂肪酸和单不饱和脂肪酸均减少。相比之下,所有样品中多不饱和脂肪酸随储存期延长而增加。相关性分析表明,风味化合物与脂肪酸、电子鼻及感官特征之间呈正相关。