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纤维质量分数对真空辅助浸渍热压成型制备的二维CF-GO/EP复合材料微观结构及性能的影响

Effect of Fiber Mass Fraction on Microstructure and Properties of 2D CF-GO/EP Composite Prepared by VIHPS.

作者信息

Ma Yuqin, Chen Yi, Li Fei, Xu Yiren, Xu Wei, Zhao Yatao, Guo Haiyin, Li Yatao, Yang Zedu, Xu Yi

机构信息

State Key Laboratory of Public Big Data, Guizhou University, Guiyang 550025, China.

School of Mechano-Electronic Engineering, Xidian University, Xi'an 710071, China.

出版信息

Nanomaterials (Basel). 2022 Apr 1;12(7):1184. doi: 10.3390/nano12071184.

Abstract

Graphene is often used to improve interlaminar fracture toughness of carbon fiber/epoxy resin (CF/EP) composites. It is still a challenge to improve the toughness while maintaining the in-layer properties. In this study, 2D graphene oxide carbon fiber reinforced epoxy resin matrix (2D CF-GO/EP) composites were prepared by a vacuum infiltration hot-press forming experimental system (VIHPS), and three-point flexural and end notch flexural (ENF) tests were carried out. With the increase of the fiber mass fraction in the composites, the mode II interlaminar fracture toughness () layers decrease gradually, and the bond property between the fiber and matrix interface layer becomes worse, because the accumulation of dense fiber bundles reduces the matrix penetration ability of cracks. However, the flexural properties increased first and then decreased, and reached the best flexural properties at 64.9%. When the fiber mass fraction is too high, the interlamellar bonding properties will decrease, and the fiber bundles will compress and affect each other. The delamination phenomenon will occur between the layers of the composites, which affects the overall bearing strength and stress limit of the composites. The results of the study show that the composites prepared by VIHPS have excellent mechanical properties, and the content of carbon fiber plays an important role in the influencing factors of the interlaminar and in-layer properties of composites.

摘要

石墨烯常用于提高碳纤维/环氧树脂(CF/EP)复合材料的层间断裂韧性。在保持层内性能的同时提高韧性仍然是一个挑战。在本研究中,通过真空浸渍热压成型实验系统(VIHPS)制备了二维氧化石墨烯碳纤维增强环氧树脂基(2D CF-GO/EP)复合材料,并进行了三点弯曲和端部切口弯曲(ENF)试验。随着复合材料中纤维质量分数的增加,II型层间断裂韧性()层逐渐降低,纤维与基体界面层之间的粘结性能变差,因为致密纤维束的堆积降低了裂纹的基体穿透能力。然而,弯曲性能先增加后降低,在64.9%时达到最佳弯曲性能。当纤维质量分数过高时,层间粘结性能会下降,纤维束会相互挤压并产生影响。复合材料层间会出现分层现象,影响复合材料的整体承载强度和应力极限。研究结果表明,VIHPS制备的复合材料具有优异的力学性能,碳纤维含量在复合材料层间和层内性能的影响因素中起着重要作用。

https://cdn.ncbi.nlm.nih.gov/pmc/blobs/8e40/9000562/9b1c067fe0ac/nanomaterials-12-01184-g001.jpg

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