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一种新型植物压榨渣钻井液降滤失剂的制备及其水凝胶性能

Preparation and Hydrogelling Performances of a New Drilling Fluid Filtrate Reducer from Plant Press Slag.

作者信息

Long Wenjun, Zhu Xialei, Zhou Fengshan, Yan Zhen, Evelina Amutenya, Liu Jinliang, Wei Zhongjin, Ma Liang

机构信息

Beijing Key Laboratory of Materials Utilization of Nonmetallic Minerals and Solid Wastes, National Laboratory of Mineral Materials, School of Materials Science and Technology, China University of Geosciences (Beijing), No. 29 Xueyuan Road, Haidian District, Beijing 100083, China.

Goldwind Environmental Protection Co., Ltd., No. 26 Kechuang 13th Street, Daxing District, Beijing 100176, China.

出版信息

Gels. 2022 Mar 23;8(4):201. doi: 10.3390/gels8040201.

DOI:10.3390/gels8040201
PMID:35448102
原文链接:https://pmc.ncbi.nlm.nih.gov/articles/PMC9028369/
Abstract

Plant press slag (PPS) containing abundant cellulose and starch is a byproduct in the deep processing of fruits, cereals, and tuberous crops products. PPS can be modified by using caustic soda and chloroacetic acid to obtain an inexpensive and environmentally friendly filtrate reducer of drilling fluids. The optimum mass ratio of m:m:m is 1:1:2, the optimum etherification temperature is 75 °C, and the obtained product is a natural mixture of carboxymethyl cellulose and carboxymethyl starch (CMCS). PPS and CMCS are characterized by using X-ray diffraction, scanning electron microscopy, Fourier transform infrared spectroscopy, thermogravimetric, X-ray photoelectron spectroscopy, and elemental analysis. The filtration loss performance of CMCS is stable before and after hot-rolling aging at 120 °C in 4.00% NaCl and saturated NaCl brine base slurry. The minimum filtration loss value of CMCS is 5.28 mL/30 min at the dosage of 1.50%. Compared with the commercial filtrate reducers with a single component, i.e., carboxymethyl starch (CMS) and low viscosity sodium carboxymethyl cellulose (LV-CMC), CMCS have a better tolerance to high temperature of 120 °C and high concentration of NaCl. The filtration loss performance of low-cost CMCS can reach the standards of LV-CMC and CMS of the specification of water-based drilling fluid materials in petroleum industry.

摘要

植物压榨渣（PPS）富含纤维素和淀粉，是水果、谷物和块茎类作物产品深加工过程中的副产品。通过使用烧碱和氯乙酸对PPS进行改性，可获得一种廉价且环保的钻井液降滤失剂。最佳质量比为m:m:m = 1:1:2，最佳醚化温度为75℃，所得产物为羧甲基纤维素和羧甲基淀粉（CMCS）的天然混合物。采用X射线衍射、扫描电子显微镜、傅里叶变换红外光谱、热重分析、X射线光电子能谱和元素分析等手段对PPS和CMCS进行了表征。在4.00% NaCl和饱和NaCl盐水基浆中，120℃热滚老化前后，CMCS的降滤失性能稳定。在加量为1.50%时，CMCS的最低滤失量值为5.28 mL/30 min。与单一组分的商业降滤失剂，即羧甲基淀粉（CMS）和低粘羧甲基纤维素（LV-CMC）相比，CMCS对120℃高温和高浓度NaCl具有更好的耐受性。低成本CMCS的降滤失性能可达到石油行业水基钻井液材料规范中LV-CMC和CMS的标准。

https://cdn.ncbi.nlm.nih.gov/pmc/blobs/c3b6/9028369/df5893a193ed/gels-08-00201-g012.jpg
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https://cdn.ncbi.nlm.nih.gov/pmc/blobs/c3b6/9028369/df5893a193ed/gels-08-00201-g012.jpg
https://cdn.ncbi.nlm.nih.gov/pmc/blobs/c3b6/9028369/4faa9bb75196/gels-08-00201-g001.jpg
https://cdn.ncbi.nlm.nih.gov/pmc/blobs/c3b6/9028369/1783c48a2314/gels-08-00201-g002.jpg
https://cdn.ncbi.nlm.nih.gov/pmc/blobs/c3b6/9028369/be6a9c9ece58/gels-08-00201-g003.jpg
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https://cdn.ncbi.nlm.nih.gov/pmc/blobs/c3b6/9028369/e19b55690564/gels-08-00201-g008.jpg
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https://cdn.ncbi.nlm.nih.gov/pmc/blobs/c3b6/9028369/df5893a193ed/gels-08-00201-g012.jpg

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