Bellaire Daniel, Thielen Stefan, Burkhart Christoph, Münnemann Kerstin, Hasse Hans, Sauer Bernd
Laboratory of Engineering Thermodynamics (LTD), TU Kaiserslautern, Kaiserslautern, Rhineland-Palatinate 67663, Germany.
Institute of machine elements, gears & transmissions (MEGT), TU Kaiserslautern, Kaiserslautern, Rhineland-Palatinate 67663, Germany.
ACS Omega. 2022 Mar 31;7(14):11671-11677. doi: 10.1021/acsomega.1c06521. eCollection 2022 Apr 12.
Compatibility between the rubber material of radial shaft seals and the lubricants to be sealed is an important requirement that customers demand of their lubricant suppliers. Among other effects that may result from incompatibility, the penetration of lubricant components into the rubber (swelling) can impair the seal's functionality due to changes in its geometry and mechanical behavior. Typically, the penetration of a lubricant into an elastomer is evaluated after an immersion test using volumetric, gravimetric, and extraction measurements. Due to the small changes that need to be detected, such methods may not be sufficient to obtain meaningful results. In this contribution, we use magnetic resonance imaging (MRI) to investigate swelling on special tribometer samples as well as a radial shaft seal that were previously used in component tests. Several combinations of rubbers and lubricants that have proven to be compatible were tested in addition to combinations with expected incompatibilities in real applications. The results indicate that MRI measurements can be used to quantify the penetration depth and potentially also the velocity with which the lubricant diffuses into the rubber, thereby yielding detailed insights into the swelling process of the seal.
径向轴封橡胶材料与待密封润滑剂之间的兼容性是客户对其润滑剂供应商提出的一项重要要求。不相容可能导致的其他影响中,润滑剂成分渗入橡胶(溶胀)会因密封件几何形状和机械性能的变化而损害其功能。通常,在浸泡试验后使用体积法、重量法和萃取测量来评估润滑剂向弹性体中的渗入情况。由于需要检测的变化很小,这些方法可能不足以获得有意义的结果。在本论文中,我们使用磁共振成像(MRI)来研究特殊摩擦计样品以及先前在部件测试中使用过的径向轴封的溶胀情况。除了在实际应用中预期不相容的组合外,还测试了几种已证明兼容的橡胶和润滑剂组合。结果表明,MRI测量可用于量化渗透深度,甚至可能量化润滑剂扩散到橡胶中的速度,从而深入了解密封件的溶胀过程。