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多层(TiAlCrSiY)N/(TiAlCr)N、单层(TiAlCrSiY)N涂层及硅在循环纳米压痕变形过程中的损伤累积现象

Damage Accumulation Phenomena in Multilayer (TiAlCrSiY)N/(TiAlCr)N, Monolayer (TiAlCrSiY)N Coatings and Silicon upon Deformation by Cyclic Nanoindentation.

作者信息

Kovalev Anatoly I, Vakhrushev Vladimir O, Beake Ben D, Konovalov Egor P, Wainstein Dmitry L, Dmitrievskii Stanislav A, Fox-Rabinovich German S, Veldhuis Stephen

机构信息

State Scientific Centre, I.P. Bardin Central Research Institute for Ferrous Metallurgy, 23/9 bdg, 2, Radio Str., 105005 Moscow, Russia.

Surface Phenomena Researches Group, LLC, Staropimenovsky Lane, 6, bdg. 1, off. 4, 127006 Moscow, Russia.

出版信息

Nanomaterials (Basel). 2022 Apr 11;12(8):1312. doi: 10.3390/nano12081312.

DOI:10.3390/nano12081312
PMID:35458020
原文链接:https://pmc.ncbi.nlm.nih.gov/articles/PMC9026849/
Abstract

The micromechanism of the low-cycle fatigue of mono- and multilayer PVD coatings on cutting tools was investigated. Multilayer nanolaminate (TiAlCrSiY)N/(TiAlCr)N and monolayer (TiAlCrSiY)N PVD coatings were deposited on the cemented carbide ball nose end mills. Low-cycle fatigue resistance was studied using the cyclic nanoindentation technique. The obtained results were compared with the behaviour of the polycrystalline silicon reference sample. The fractal analysis of time-resolved curves for indenter penetration depth demonstrated regularities of damage accumulation in the coatings at the early stage of wear. The difference in low-cycle fatigue of the brittle silicon and nitride wear-resistant coatings is shown. It is demonstrated that when distinguished from the single layer (TiAlCrSiY)N coating, the nucleation and growth of microcracks in the multilayer (TiAlCrSiY)N/(TiAlCr)N coating is accompanied by acts of microplastic deformation providing a higher fracture toughness of the multilayer nanolaminate (TiAlCrSiY)N/(TiAlCr)N.

摘要

研究了切削刀具上单层和多层物理气相沉积(PVD)涂层的低周疲劳微观机制。在硬质合金球头立铣刀上沉积了多层纳米层状结构(TiAlCrSiY)N/(TiAlCr)N和单层(TiAlCrSiY)N物理气相沉积涂层。使用循环纳米压痕技术研究了低周疲劳抗力。将所得结果与多晶硅参考样品的行为进行了比较。对压头穿透深度的时间分辨曲线进行分形分析,揭示了涂层在磨损早期损伤积累的规律。展示了脆性硅和氮化物耐磨涂层在低周疲劳方面的差异。结果表明,与单层(TiAlCrSiY)N涂层不同,多层(TiAlCrSiY)N/(TiAlCr)N涂层中微裂纹的形核和扩展伴随着微塑性变形行为,这使得多层纳米层状结构(TiAlCrSiY)N/(TiAlCr)N具有更高的断裂韧性。

https://cdn.ncbi.nlm.nih.gov/pmc/blobs/7ff3/9026849/caf9539a713f/nanomaterials-12-01312-g004.jpg
https://cdn.ncbi.nlm.nih.gov/pmc/blobs/7ff3/9026849/fe5bddf3237a/nanomaterials-12-01312-g001.jpg
https://cdn.ncbi.nlm.nih.gov/pmc/blobs/7ff3/9026849/dd4f93a4ccdf/nanomaterials-12-01312-g002.jpg
https://cdn.ncbi.nlm.nih.gov/pmc/blobs/7ff3/9026849/6a297c0975a7/nanomaterials-12-01312-g003.jpg
https://cdn.ncbi.nlm.nih.gov/pmc/blobs/7ff3/9026849/caf9539a713f/nanomaterials-12-01312-g004.jpg
https://cdn.ncbi.nlm.nih.gov/pmc/blobs/7ff3/9026849/fe5bddf3237a/nanomaterials-12-01312-g001.jpg
https://cdn.ncbi.nlm.nih.gov/pmc/blobs/7ff3/9026849/dd4f93a4ccdf/nanomaterials-12-01312-g002.jpg
https://cdn.ncbi.nlm.nih.gov/pmc/blobs/7ff3/9026849/6a297c0975a7/nanomaterials-12-01312-g003.jpg
https://cdn.ncbi.nlm.nih.gov/pmc/blobs/7ff3/9026849/caf9539a713f/nanomaterials-12-01312-g004.jpg

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本文引用的文献

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