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美国国家标准与技术研究院的小角中子散射仪。

The very small angle neutron scattering instrument at the National Institute of Standards and Technology.

作者信息

Barker John, Moyer James, Kline Steven, Jensen Grethe, Cook Jeremy, Gagnon Cedric, Kelley Elizabeth, Chabot Jean Philippe, Maliszewskyj Nicholas, Parikh Chirag, Chen Wangchun, Murphy R P, Glinka Charles

机构信息

NIST Center for Neutron Research, National Institute of Standards and Technology, 100 Bureau Drive, Stop 6102, Gaithersbug, MD 20899, USA.

Danish Technological Institute, Gregersensvej, Taastrup DK-2630, Denmark.

出版信息

J Appl Crystallogr. 2022 Feb 27;55(Pt 2):271-283. doi: 10.1107/S1600576722000826. eCollection 2022 Apr 1.

Abstract

A description and the performance of the very small angle neutron scattering diffractometer at the National Institute of Standards and Technology are presented. The measurement range of the instrument extends over three decades of momentum transfer from 2 × 10 to 0.7 Å. The entire scattering angle range from 8 × 10 to π/6 rad (30°) can be measured simultaneously using three separate detector carriages on rails holding nine 2D detector arrays. Versatile choices of collimation options and neutron wavelength selection allow the resolution and beam intensity to be optimized for the needs of the experiment. High resolution is achieved using multiple converging-beam collimation with circular pinholes combined with refractive lenses and prisms. Relaxed vertical resolution with much higher beam intensity can be achieved with narrow slit collimation and a broad wavelength range chosen by truncating the moderator source distribution below 4 Å with a Be crystalline filter and above 8 Å with a supermirror deflector. Polarized beam measurements with full polarization analysis are also provided by a high-performance supermirror polarizer and spin flipper, capable of producing flipping ratios of over 100, along with a high-efficiency He polarization analyzer.

摘要

介绍了美国国家标准与技术研究院的小角中子散射衍射仪的相关描述及性能。该仪器的测量范围涵盖了动量转移的三个数量级,从2×10至0.7 Å。使用安装在轨道上的三个独立探测器滑架,每个滑架装有九个二维探测器阵列,可同时测量从8×10至π/6 rad(30°)的整个散射角范围。准直选项和中子波长选择的多种组合,可根据实验需求优化分辨率和光束强度。通过使用带有圆形针孔的多个会聚束准直,并结合折射透镜和棱镜,可实现高分辨率。通过窄缝准直以及使用铍晶体滤波器在4 Å以下截断慢化剂源分布、使用超镜偏转器在8 Å以上截断慢化剂源分布来选择较宽的波长范围,可实现具有更高光束强度的宽松垂直分辨率。高性能超镜偏振器和自旋翻转器还可提供具有全偏振分析的偏振光束测量,其能够产生超过100的翻转比,同时配备高效的氦偏振分析仪。

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