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不同有机酸提取的沃柑(Clausena lansium (Lour.) Skeels)果皮果胶的理化性质、结构和功能特性。

Physicochemical, structural, and functional properties of wampee (Clausena lansium (Lour.) Skeels) fruit peel pectin extracted with different organic acids.

机构信息

Sericultural & Argi-Food Research Institute, Guangdong Academy of Agricultural Sciences/Key Laboratory of Functional Foods, Ministry of Agriculture and Rural Affairs/Guangdong Key Laboratory of Agricultural Products Processing, No. 133 Yiheng Street, Dongguanzhuang Road, Tianhe District, Guangzhou 510610, China.

School of Public Health, Southern Medical University, Guangzhou 510610, China.

出版信息

Food Chem. 2022 Aug 30;386:132834. doi: 10.1016/j.foodchem.2022.132834. Epub 2022 Apr 4.

Abstract

Effects of different extraction acids on physicochemical, structural, and functional properties of wampee fruit peel pectin (WFPP) were comparatively investigated. The hydrochloric acid extracted WFPP (HEP) exhibited the highest degrees of methylation (67.79%) and acetylation (86.29%) coupling with abundant monosaccharides and rhamnogalacturonan branches, but lowest molecular weight (5.58 × 10 Da). The results of SEM, X-ray diffraction, and Fourier transform infrared spectroscopy analyses showed that acid types had little effect on the surface morphology of WFPP. However, compared to commercial citrus pectin (CCP), several specific absorbance peaks (1539, 1019, 920 cm) were found in WFPPs, which corresponds to aromatic skeletal stretching, pyranose, and d-glucopyranosyl, respectively. Moreover, the rheological behavior revealed that WFPP solution was pseudoplastic fluid and affected by acid types. And the WFPPs exhibited higher emulsifying activity and emulsion stability than CCP. All these WFPPs presented well antioxidant activity and promoting probiotics ability, especially for HEP.

摘要

比较了不同提取酸对山竹果皮果胶(WFPP)理化性质、结构和功能特性的影响。盐酸提取的 WFPP(HEP)具有最高的甲氧基化(67.79%)和乙酰化(86.29%)程度,与丰富的单糖和鼠李半乳糖醛酸支链偶联,但分子量最低(5.58×10 Da)。SEM、X 射线衍射和傅里叶变换红外光谱分析的结果表明,酸的类型对 WFPP 的表面形态几乎没有影响。然而,与商业柑橘果胶(CCP)相比,在 WFPP 中发现了几个特定的吸收峰(1539、1019、920 cm),分别对应于芳族骨架拉伸、吡喃糖和 d-吡喃葡萄糖基。此外,流变行为表明,WFPP 溶液是假塑性流体,并受酸类型的影响。并且 WFPP 比 CCP 具有更高的乳化活性和乳液稳定性。所有这些 WFPP 都表现出良好的抗氧化活性和促进益生菌能力,特别是对于 HEP。

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