Mahmood Sultan, Iqbal Amjad, Wadood Abdul, Mateen Abdul, Amin Muhammad, Yahia Ibrahim S, Zahran Heba Y
Department of Materials Science and Engineering, Institute of Space Technology, Islamabad 44000, Pakistan.
Department of Materials Technologies, Faculty of Materials Engineering, Silesian University of Technology, Gliwice 44-100, Poland.
Molecules. 2022 Apr 21;27(9):2666. doi: 10.3390/molecules27092666.
In the present work, 0.25 wt%GNP-Ti composites were prepared through powder metallurgy route by adopting three types of mixing modes to investigate the extent of mixing on the mechanical and tribological properties. Dry ball milling, wet ball milling, and rotator mixing were independently employed to homogenize the composite constituents. Three types of composite powders obtained were subsequently sintered into composite pellets by cold compaction followed by vacuum sintering. Morphological investigation of composite powders performed by SEM revealed better homogenization of GNPs in Ti matrix for dry ball milled composite powder, whereas wet ball milled and rotator mixed composite powders showed aggregation and bundling of GNPs. Micro Vickers hardness of composites produced via dry ball milling is 4.56% and 15.7% higher than wet ball milled and rotator mixed samples, respectively. Wear test performed by pin-on-disk tribometer showed higher wear loss for wet ball milled and rotator mixed composites in comparison to dry ball milled.
在本工作中,通过粉末冶金路线,采用三种混合方式制备了0.25 wt%的GNP-Ti复合材料,以研究混合程度对力学性能和摩擦学性能的影响。分别采用干球磨、湿球磨和旋转混合方式使复合成分均匀化。随后,通过冷压接着真空烧结,将获得的三种复合粉末烧结成复合颗粒。通过扫描电子显微镜(SEM)对复合粉末进行的形态学研究表明,对于干球磨复合粉末,GNPs在Ti基体中的均匀化程度更好,而湿球磨和旋转混合复合粉末则显示出GNPs的团聚和束集现象。通过干球磨制备的复合材料的显微维氏硬度分别比湿球磨和旋转混合样品高4.56%和15.7%。通过销盘摩擦计进行的磨损试验表明,与干球磨复合材料相比,湿球磨和旋转混合复合材料的磨损损失更高。