Zhang Guodong, Liu Wei, Zhang Peng, Xiong Huaping, Gao Jianshi, Yu Huai, Yuan Hong
3D Printing Research & Engineering Technology Center, Beijing Institute of Aeronautical Materials, Beijing 100095, China.
Materials (Basel). 2022 Apr 25;15(9):3109. doi: 10.3390/ma15093109.
Electron beam directed energy deposition (EB-DED) is a promising manufacturing process for the fabrication of large-scale, fully dense and near net shape metallic components. However, limited knowledge is available on the EB-DED process of titanium alloys. In this study, a near-α high-temperature titanium alloy Ti60 (Ti-5.8Al-4Sn-4Zr-0.7Nb-1.5Ta-0.4Si) was fabricated via EB-DED. The chemical composition, microstructure, tensile property (at room temperature and 600 °C), and creep behavior of the fabricated alloy were investigated and compared with those of the conventional wrought lamellar and bimodal counterparts. Results indicated that the average evaporation loss of Al and Sn was 10.28% and 5.01%, respectively. The microstructure of the as-built alloy was characterized by coarse columnar grains, lamellar α, and the precipitated elliptical silicides at the α/β interfaces. In terms of tensile properties, the vertical specimens exhibited lower strength but higher ductility than the horizontal specimens at both room temperature and 600 °C. Furthermore, the tensile creep strain of the EB-DED Ti60 alloy measured at 600 °C and 150 MPa for 100 h under as-built and post-deposition STA conditions was less than 0.15%, which meets the standard requirements for the wrought Ti60 alloy. The creep resistance of the EB-DED Ti60 alloy was superior to that of its wrought bimodal counterpart.
电子束定向能量沉积(EB-DED)是一种用于制造大型、全致密和近净形金属部件的有前途的制造工艺。然而,关于钛合金的EB-DED工艺的知识有限。在本研究中,通过EB-DED制备了一种近α型高温钛合金Ti60(Ti-5.8Al-4Sn-4Zr-0.7Nb-1.5Ta-0.4Si)。对制备合金的化学成分、微观结构、拉伸性能(室温及600℃)和蠕变行为进行了研究,并与传统锻造的片状和双峰组织的对应物进行了比较。结果表明,Al和Sn的平均蒸发损失分别为10.28%和5.01%。增材制造态合金的微观结构特征为粗大的柱状晶粒、片状α相以及在α/β界面处析出的椭圆形硅化物。在拉伸性能方面,垂直试样在室温及600℃下均表现出比水平试样更低的强度但更高的延展性。此外,在增材制造态和沉积后STA条件下,EB-DED Ti60合金在600℃和150 MPa下测量100 h的拉伸蠕变应变小于0.15%,满足锻造Ti60合金的标准要求。EB-DED Ti60合金的抗蠕变性能优于其锻造双峰组织的对应物。