Li Ying, Podaný Pavel, Koukolíková Martina, Džugan Jan, Krajňák Tomáš, Veselý Jozef, Raghavan Srinivasan
COMTES FHT a.s., Prumyslova 995, 334 41 Dobrany, Czech Republic.
Department of Physics of Materials, Faculty of Mathematics and Physics, Charles University, 121 16 Prague 2, Czech Republic.
Materials (Basel). 2023 Feb 6;16(4):1377. doi: 10.3390/ma16041377.
The creep properties of a laser-directed energy deposition (L-DED) technique manufactured Inconel 718 (IN718) was investigated at 650 °C/700 MPa. Microstructure and creep properties of L-DED IN718 samples were tailored by various post heat treatments involving homogenization heat treatment with temperature ranging from 1080 to 1180 °C + double aging and hot isostatic pressing (HIP). Microstructural changes and their influence on the creep behavior and fracture mechanism were observed and discussed. The results show that L-DED sample heat treated by a simple double aging exhibits a 49% increase in creep lifetime t and a comparable creep elongation ɛ when compared to the wrought material, due to the reserved coarse dislocation cell substructure from the L-DED process. The loss of dislocation cell structure and the coarsening of grains at higher temperature of heat treatments contributes to a shorter t ε, but faster ε̇ (minimum creep rate). The present work demonstrates that a simultaneous improvement of creep strength and creep elongation can be achieved in the case of a coarse-grained L-DED IN718 by a double aging treatment which can preserve both the strengthening precipitates and an appropriate size of dislocation cells.
研究了激光定向能量沉积(L-DED)技术制造的Inconel 718(IN718)在650°C/700MPa下的蠕变性能。通过各种后热处理来调整L-DED IN718样品的微观结构和蠕变性能,这些后热处理包括温度范围为1080至1180°C的均匀化热处理+双重时效和热等静压(HIP)。观察并讨论了微观结构变化及其对蠕变行为和断裂机制的影响。结果表明,与锻造材料相比,通过简单双重时效热处理的L-DED样品的蠕变寿命t增加了49%,蠕变伸长率ɛ相当,这是由于L-DED过程中保留了粗大的位错胞亚结构。在较高热处理温度下位错胞结构的丧失和晶粒的粗化导致t和ɛ缩短,但ɛ̇(最小蠕变速率)更快。目前的工作表明,对于粗晶粒的L-DED IN718,通过双重时效处理可以同时提高蠕变强度和蠕变伸长率,该处理可以保留强化析出相和适当尺寸的位错胞。