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粉末冶金和T6热处理制备的SiC/AA2024纳米复合材料的微观结构与力学性能研究

Investigation of Microstructures and Mechanical Properties of SiC/AA2024 Nanocomposites Processed by Powder Metallurgy and T6 Heat Treatment.

作者信息

Mu Dikunqi, Zhang Zhen, Liang Jiamiao, Wang Jun, Zhang Deliang

机构信息

Shanghai Key Lab of Advanced High-Temperature Materials, Precision Forming and State Key Lab of Metal Matrix Composites, Shanghai Jiao Tong University, Shanghai 200240, China.

State Key Laboratory of Rolling and Automation, Northeastern University, Shenyang 110819, China.

出版信息

Materials (Basel). 2022 May 16;15(10):3547. doi: 10.3390/ma15103547.

Abstract

SiC/AA2024 nanocomposites with 1 and 5 vol.% SiC nanoparticles have been prepared by a powder metallurgy route involving high-energy ball-milling (HEBM), spark plasma sintering (SPS), and hot extrusion. The microstructures and mechanical properties of the nanocomposite samples before and after T6 heat treatment were investigated. The samples exhibited a bimodal microstructure with SiC nanoparticles being dispersed in it. With increasing the SiC nanoparticle content from 1 to 5 vol.%, the yield strength (YS) and ultimate tensile strength (UTS) increased and the elongation to fracture (El) slightly decreased. After T6 heat treatment, a simultaneous improvement of the strength and ductility was observed, with the YS, UTS, and El increasing from 413 MPa, 501 MPa, and 5.4% to 496 MPa, 572 MPa, and 6.7%, respectively, in the 1 vol.%SiC/AA2024 nanocomposite sample. Analysis of the deformation behavior shows that this improvement is likely caused by the increased density of geometrically necessary dislocations (GNDs) resulting from the bimodal microstructure. The dispersed intragranular S' precipitates generated by the T6 heat treatment also make a contribution to the increase of strength and ductility by accumulating dislocations. It is feasible to realize simultaneous improvement of strength and ductility in the SiC/AA2024 nanocomposites via powder metallurgy and subsequent heat treatment.

摘要

通过高能球磨(HEBM)、放电等离子烧结(SPS)和热挤压的粉末冶金路线制备了含有1体积%和5体积%碳化硅纳米颗粒的SiC/AA2024纳米复合材料。研究了T6热处理前后纳米复合材料样品的微观结构和力学性能。样品呈现出双峰微观结构,其中碳化硅纳米颗粒分散在其中。随着碳化硅纳米颗粒含量从1体积%增加到5体积%,屈服强度(YS)和极限抗拉强度(UTS)增加,断裂伸长率(El)略有下降。T6热处理后,强度和延展性同时得到改善,在1体积%SiC/AA2024纳米复合材料样品中,YS、UTS和El分别从413MPa、501MPa和5.4%增加到496MPa、572MPa和6.7%。对变形行为的分析表明,这种改善可能是由于双峰微观结构导致的几何必要位错(GNDs)密度增加所致。T6热处理产生的弥散晶内S'析出物也通过积累位错对强度和延展性的增加做出了贡献。通过粉末冶金和后续热处理实现SiC/AA2024纳米复合材料强度和延展性的同时提高是可行的。

https://cdn.ncbi.nlm.nih.gov/pmc/blobs/9cdb/9145340/916afdedc05f/materials-15-03547-g001a.jpg

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