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7085铝合金熔体的超声弯曲振动辅助净化实验研究

Ultrasonic Bending Vibration-Assisted Purification Experimental Study of 7085 Aluminum Alloy Melt.

作者信息

Shi Chen, He Jiangnan, Liao Hua, Mao Daheng

机构信息

Light Alloy Research Institute, Central South University, Changsha 410083, China.

State Key Laboratory of High Performance Complex Manufacturing, Central South University, Changsha 410083, China.

出版信息

Materials (Basel). 2022 May 18;15(10):3598. doi: 10.3390/ma15103598.

DOI:10.3390/ma15103598
PMID:35629624
原文链接:https://pmc.ncbi.nlm.nih.gov/articles/PMC9144351/
Abstract

Aiming at the problem that melt inclusions in the casting process of 7085 aluminum alloy seriously affect the ingot quality, this study introduces ultrasonic bending vibration into the melt of the launder in the semi-continuous casting process of 7085 aluminum alloy and investigates the online purification effect of ultrasonic bending vibration on the melt of 7085 aluminum alloy through a metallographic analysis, SEM analysis, and EDS energy spectrum analysis. The results show that, under the action of the ultrasonic, the inclusions in the aluminum melt are transformed from a large number of elongated large inclusions with a size of more than 50 μm, and granular inclusions with a size of about 5-15 μm, into a small amount of smaller than 30 μm point-like small inclusions. In addition, the average area ratio of inclusions in the melted sample was reduced from 3.835 (±0.05)% to 0.458 (±0.05)%, and the residual refining agent in the aluminum melt was effectively removed. It was also found that under the action of ultrasonic bending vibration, the tiny inclusions in the melt aggregate with each other, and interact with the residual refining agent in the melt to further grow, and are attached to the inner surface of the ceramic cavity channel to be removed.

摘要

针对7085铝合金铸造过程中熔体夹杂物严重影响铸锭质量的问题,本研究将超声弯曲振动引入7085铝合金半连续铸造过程中流槽的熔体中,并通过金相分析、扫描电子显微镜(SEM)分析和能谱分析研究超声弯曲振动对7085铝合金熔体的在线净化效果。结果表明,在超声作用下,铝熔体中的夹杂物由大量尺寸大于50μm的细长状大夹杂物和尺寸约为5 - 15μm的颗粒状夹杂物,转变为少量尺寸小于30μm的点状小夹杂物。此外,熔体样品中夹杂物的平均面积比从3.835(±0.05)%降至0.458(±0.05)%,铝熔体中的残留精炼剂被有效去除。还发现,在超声弯曲振动作用下,熔体中的微小夹杂物相互聚集,并与熔体中的残留精炼剂相互作用进一步长大,附着在陶瓷腔体通道内表面而被去除。

https://cdn.ncbi.nlm.nih.gov/pmc/blobs/e7d4/9144351/b41c1777cd0c/materials-15-03598-g012.jpg
https://cdn.ncbi.nlm.nih.gov/pmc/blobs/e7d4/9144351/038163a237dd/materials-15-03598-g001.jpg
https://cdn.ncbi.nlm.nih.gov/pmc/blobs/e7d4/9144351/b13598e1c4dc/materials-15-03598-g002.jpg
https://cdn.ncbi.nlm.nih.gov/pmc/blobs/e7d4/9144351/066ccc85cb9f/materials-15-03598-g003.jpg
https://cdn.ncbi.nlm.nih.gov/pmc/blobs/e7d4/9144351/18f4bb96f86f/materials-15-03598-g004.jpg
https://cdn.ncbi.nlm.nih.gov/pmc/blobs/e7d4/9144351/c80fa3278467/materials-15-03598-g005.jpg
https://cdn.ncbi.nlm.nih.gov/pmc/blobs/e7d4/9144351/a2b8d9d36f47/materials-15-03598-g006a.jpg
https://cdn.ncbi.nlm.nih.gov/pmc/blobs/e7d4/9144351/31d9a39fa7de/materials-15-03598-g007.jpg
https://cdn.ncbi.nlm.nih.gov/pmc/blobs/e7d4/9144351/2f4d34cbe086/materials-15-03598-g008.jpg
https://cdn.ncbi.nlm.nih.gov/pmc/blobs/e7d4/9144351/ceebc5e077b3/materials-15-03598-g009.jpg
https://cdn.ncbi.nlm.nih.gov/pmc/blobs/e7d4/9144351/65140af605e2/materials-15-03598-g010.jpg
https://cdn.ncbi.nlm.nih.gov/pmc/blobs/e7d4/9144351/7ffe7e906e85/materials-15-03598-g011.jpg
https://cdn.ncbi.nlm.nih.gov/pmc/blobs/e7d4/9144351/b41c1777cd0c/materials-15-03598-g012.jpg
https://cdn.ncbi.nlm.nih.gov/pmc/blobs/e7d4/9144351/038163a237dd/materials-15-03598-g001.jpg
https://cdn.ncbi.nlm.nih.gov/pmc/blobs/e7d4/9144351/b13598e1c4dc/materials-15-03598-g002.jpg
https://cdn.ncbi.nlm.nih.gov/pmc/blobs/e7d4/9144351/066ccc85cb9f/materials-15-03598-g003.jpg
https://cdn.ncbi.nlm.nih.gov/pmc/blobs/e7d4/9144351/18f4bb96f86f/materials-15-03598-g004.jpg
https://cdn.ncbi.nlm.nih.gov/pmc/blobs/e7d4/9144351/c80fa3278467/materials-15-03598-g005.jpg
https://cdn.ncbi.nlm.nih.gov/pmc/blobs/e7d4/9144351/a2b8d9d36f47/materials-15-03598-g006a.jpg
https://cdn.ncbi.nlm.nih.gov/pmc/blobs/e7d4/9144351/31d9a39fa7de/materials-15-03598-g007.jpg
https://cdn.ncbi.nlm.nih.gov/pmc/blobs/e7d4/9144351/2f4d34cbe086/materials-15-03598-g008.jpg
https://cdn.ncbi.nlm.nih.gov/pmc/blobs/e7d4/9144351/ceebc5e077b3/materials-15-03598-g009.jpg
https://cdn.ncbi.nlm.nih.gov/pmc/blobs/e7d4/9144351/65140af605e2/materials-15-03598-g010.jpg
https://cdn.ncbi.nlm.nih.gov/pmc/blobs/e7d4/9144351/7ffe7e906e85/materials-15-03598-g011.jpg
https://cdn.ncbi.nlm.nih.gov/pmc/blobs/e7d4/9144351/b41c1777cd0c/materials-15-03598-g012.jpg

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本文引用的文献

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Effects of Ultrasonic Bending Vibration Introduced by an L-Shaped Ultrasonic Rod on the Microstructure and Properties of a 1060 Aluminum Alloy Strip Formed by Twin-Roll Casting.L形超声棒引入的超声弯曲振动对双辊铸轧1060铝合金带材组织与性能的影响
Materials (Basel). 2020 Apr 25;13(9):2013. doi: 10.3390/ma13092013.
2
Effect of Ultrasonic Bending Vibration Introduced by the L-shaped Ultrasonic Rod on Solidification Structure and Segregation of Large 2A14 Ingots.L形超声棒引入的超声弯曲振动对大型2A14铸锭凝固组织和偏析的影响
Materials (Basel). 2020 Feb 10;13(3):807. doi: 10.3390/ma13030807.
3
Fundamental studies of ultrasonic melt processing.
超声熔体处理的基础研究。
Ultrason Sonochem. 2019 Apr;52:455-467. doi: 10.1016/j.ultsonch.2018.12.028. Epub 2018 Dec 15.
4
Dual-frequency ultrasonic treatment on microstructure and mechanical properties of ZK60 magnesium alloy.ZK60镁合金微观结构与力学性能的双频超声处理
Ultrason Sonochem. 2018 Jan;40(Pt A):433-441. doi: 10.1016/j.ultsonch.2017.07.027. Epub 2017 Jul 20.