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飞秒激光处理对二硅酸锂微晶玻璃和高透氧化锆陶瓷表面形貌优化的初步研究

Preliminary Study on the Optimization of Femtosecond Laser Treatment on the Surface Morphology of Lithium Disilicate Glass-Ceramics and Highly Translucent Zirconia Ceramics.

作者信息

Inokoshi Masanao, Yoshihara Kumiko, Kakehata Masayuki, Yashiro Hidehiko, Nagaoka Noriyuki, Tonprasong Watcharapong, Xu Kaiqi, Minakuchi Shunsuke

机构信息

Department of Gerodontology and Oral Rehabilitation, Graduate School of Medical and Dental Sciences, Tokyo Medical and Dental University, Tokyo 113-8549, Japan.

National Institute of Advanced Industrial Science and Technology (AIST), Health and Medical Research Institute, Takamatsu 761-0395, Japan.

出版信息

Materials (Basel). 2022 May 18;15(10):3614. doi: 10.3390/ma15103614.

Abstract

All-ceramic restorations have become increasingly popular in dentistry. Toward ensuring that these restorations adhere to the tooth structure, this study determines the optimal femtosecond laser (FL) treatment parameters for lithium disilicate glass-ceramics and highly translucent zirconia ceramics with respect to surface morphology. For both the ceramics, the following surface conditions were investigated: (1) as-sintered; (2) AlO sandblasted; (3) FL treatment (dot pattern with line distances of 14, 20, and 40 µm); (4) FL treatment (crossed-line pattern with a line distance of 20 and 40 µm). Surface roughness parameters were estimated using a 3D confocal laser microscope; microstructures were analyzed using a scanning electron microscope. Peak fluence (F) values of 4 and 8 J/cm and irradiation numbers (N) of 20 and 10 shots were selected to create dot patterns in highly translucent zirconia and lithium disilicate glass-ceramics, respectively. Furthermore, F = 8 J/cm and N = 20 shots were chosen to obtain crossed-line patterns in both ceramics. Our results show that lithium disilicate glass-ceramics and highly translucent zirconia exhibit a similar surface morphology under each of the surface treatment conditions. Therefore, FL irradiation of dot or crossed-line patterns (at a distance of 20 and 40 µm) are potential candidates for future investigations.

摘要

全瓷修复体在牙科领域越来越受欢迎。为确保这些修复体与牙齿结构紧密结合,本研究针对二硅酸锂玻璃陶瓷和高透明度氧化锆陶瓷,就表面形态确定了最佳飞秒激光(FL)处理参数。对于这两种陶瓷,研究了以下表面条件:(1)烧结态;(2)用AlO喷砂处理;(3)飞秒激光处理(点图案,线间距为14、20和40 µm);(4)飞秒激光处理(交叉线图案,线间距为20和40 µm)。使用三维共聚焦激光显微镜估计表面粗糙度参数;用扫描电子显微镜分析微观结构。分别选择4和8 J/cm的峰值能量密度(F)值以及20和10次的照射次数(N),在高透明度氧化锆和二硅酸锂玻璃陶瓷中制作点图案。此外,选择F = 8 J/cm和N = 20次照射,在两种陶瓷中获得交叉线图案。我们的结果表明,在每种表面处理条件下,二硅酸锂玻璃陶瓷和高透明度氧化锆呈现出相似的表面形态。因此,飞秒激光照射的点图案或交叉线图案(线间距为20和40 µm)是未来研究的潜在对象。

https://cdn.ncbi.nlm.nih.gov/pmc/blobs/ed49/9143866/8e26bb27b2f8/materials-15-03614-g001.jpg

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