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热处理Ti-6Al-7Nb牙科合金的力学性能和腐蚀行为

Mechanical Properties and Corrosion Behavior of Thermally Treated Ti-6Al-7Nb Dental Alloy.

作者信息

Hulka Iosif, Florido-Suarez Nestor R, Mirza-Rosca Julia C, Saceleanu Adriana

机构信息

Department of Mechanical Engineering, Las Palmas de Gran Canaria University, 35017 Las Palmas de Gran Canaria, Spain.

Medicine Faculty, Lucian Blaga University of Sibiu, 550024 Sibiu, Romania.

出版信息

Materials (Basel). 2022 May 27;15(11):3813. doi: 10.3390/ma15113813.

Abstract

Ti and its alloys have the most satisfactory properties for biomedical applications due to their specific strength, high corrosion resistance, and high biocompatibility. Ti-6Al-7Nb has been approved for clinical use, proving to be a viable replacement for the Ti-6Al-4V alloy that has been used for many decades in medical applications. In our study, the Ti-6Al-7Nb alloy underwent heat treatment, was cooled in various cooling media such as mineral oil and water, and was then quenched in the oven. The microstructure was investigated, and the mechanical characterization was carried out by Vickers microhardness test. Young's modulus measurements and tensile tests were performed in order to study the effect of cooling media on the material. To study the corrosion behavior, in vitro studies were performed on the Ti-6Al-7Nb samples in simulated body conditions by using artificial saliva. It was observed that the martensitic phase changed as a function of cooling media, and a less intensive cooling medium decreases strength properties' indicators as well as hardness values. The results emphasize that the use of heat treatment improves the passive layer's resistance in the presence of artificial saliva.

摘要

钛及其合金因其比强度、高耐腐蚀性和高生物相容性,在生物医学应用中具有最令人满意的性能。Ti-6Al-7Nb已被批准用于临床,事实证明它是在医疗应用中已使用数十年的Ti-6Al-4V合金的可行替代品。在我们的研究中,对Ti-6Al-7Nb合金进行了热处理,在矿物油和水等各种冷却介质中冷却,然后在烤箱中淬火。研究了其微观结构,并通过维氏显微硬度测试进行了力学表征。进行了杨氏模量测量和拉伸试验,以研究冷却介质对材料的影响。为了研究腐蚀行为,在模拟人体条件下,使用人工唾液对Ti-6Al-7Nb样品进行了体外研究。观察到马氏体相随冷却介质而变化,冷却介质强度较低会降低强度性能指标以及硬度值。结果强调,热处理的使用提高了在人工唾液存在下钝化层的抗性。

https://cdn.ncbi.nlm.nih.gov/pmc/blobs/f6f0/9181047/63e8362f8b20/materials-15-03813-g001.jpg

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