Zhou Chuankun, Cao Fang, Yang Zhirong, Rao Weifeng
School of Mechanical Engineering, Qilu University of Technology (Shandong Academy of Sciences), Jinan 250353, China.
Shandong Institute of Mechanical Design and Research, Jinan 250353, China.
Materials (Basel). 2024 Mar 29;17(7):1572. doi: 10.3390/ma17071572.
The mechanical properties of metastable β-titanium alloys are highly susceptible during the thermal mechanical processing (TMP). In this process, the recrystallization process plays an important role in determining the microstructure and texture evolution. The implementation of dynamic recrystallization (DRX), a process for achieving β-grain refinement, is considered of great significance for the improvement of the properties of metastable β-titanium alloys and their industrial production. Along these lines, in this work, an isothermal compression test of TB8 titanium alloy was carried out by using a Gleeble-3500 thermal simulator. As a result, the rheological stress behavior was analyzed, the thermal processing map was accurately established based on the stress-strain curve, and the optimal processing interval was determined. The DRX kinetic and the DRX grain size models were developed, on the basis of which a new DRX intrinsic model was established to improve the material parameters. Therefore, the actual situation in the working process could be better predicted. The microstructural evolution of TB8 titanium alloy during thermal deformation was comprehensively investigated using the electron backscatter diffraction (EBSD) technique. The obtained results demonstrate a close correlation between the diversity of DRX mechanisms in TB8 alloy and the distribution of dislocation density. Four microstructural textures during thermal deformation were identified, in which the cube texture of (001) <010> and the R-Gorss Nd texture of (110) <110> dominate. Due to the random orientation of the dynamically recrystallized grains, the strength of the R-Gorss Nd texture of (110) <110> increases with the increase in the volume fraction of DRX. On the contrary, it was verified that the dynamic recrystallization behavior has a significant weakening impact on the cube texture of (001) <010>.
亚稳β钛合金的力学性能在热机械加工(TMP)过程中高度敏感。在此过程中,再结晶过程在决定微观结构和织构演变方面起着重要作用。动态再结晶(DRX)作为一种实现β晶粒细化的过程,其实施对于改善亚稳β钛合金的性能及其工业生产具有重要意义。基于此,在本工作中,使用Gleeble-3500热模拟机对TB8钛合金进行了等温压缩试验。结果,分析了流变应力行为,基于应力-应变曲线精确建立了热加工图,并确定了最佳加工区间。建立了DRX动力学和DRX晶粒尺寸模型,在此基础上建立了一个新的DRX本征模型以改进材料参数。因此,可以更好地预测工作过程中的实际情况。利用电子背散射衍射(EBSD)技术全面研究了TB8钛合金在热变形过程中的微观结构演变。所得结果表明,TB8合金中DRX机制的多样性与位错密度分布之间存在密切相关性。识别出了热变形过程中的四种微观结构织构,其中(001)<010>的立方织构和(110)<110>的R-Gorss Nd织构占主导。由于动态再结晶晶粒的取向随机,(110)<110>的R-Gorss Nd织构强度随DRX体积分数的增加而增加。相反,已证实动态再结晶行为对(001)<010>的立方织构有显著的弱化影响。