Deng Bo, Dai Yilong, Lin Jianguo, Zhang Dechuang
School of Materials Science and Engineering, Xiangtan University, Xiangtan 411105, China.
Key Laboratory of Materials Design and Preparation Technology of Hunan Province, Xiangtan University, Xiangtan 411105, China.
Materials (Basel). 2022 Jun 3;15(11):3985. doi: 10.3390/ma15113985.
Magnesium alloys show broad application prospects as biodegradable implanting materials due to their good biocompatibility, mechanical compatibility, and degradability. However, the influence mechanism of microstructure evolution during forming on the mechanical properties and corrosion resistance of the magnesium alloy process is not clear. Here, the effects of rolling deformation, such as cold rolling, warm rolling, and hot rolling, on the microstructure, mechanical properties, and corrosion resistance of the WE43 magnesium alloy were systematically studied. After rolling treatment, the grains of the alloy were significantly refined. Moreover, the crystal plane texture strength and basal plane density decreased first and then increased with the increase in rolling temperature. Compared with the as-cast alloy, the strength of the alloy after rolling was significantly improved. Among them, the warm-rolled alloy exhibited the best mechanical properties, with a tensile strength of 346.7 MPa and an elongation of 8.9%. The electrochemical experiments and immersion test showed that the hot working process can greatly improve the corrosion resistance of the WE43 alloy. The hot-rolled alloy had the best corrosion resistance, and its corrosion resistance rate was 0.1556 ± 0.18 mm/year.
镁合金因其良好的生物相容性、力学相容性和可降解性,作为可生物降解植入材料展现出广阔的应用前景。然而,镁合金加工过程中成形时微观结构演变对其力学性能和耐腐蚀性的影响机制尚不清楚。在此,系统研究了冷轧、温轧和热轧等轧制变形对WE43镁合金微观结构、力学性能和耐腐蚀性的影响。轧制处理后,合金晶粒显著细化。此外,晶体平面织构强度和基面密度随轧制温度升高先降低后升高。与铸态合金相比,轧制后合金的强度显著提高。其中,温轧合金表现出最佳力学性能,抗拉强度为346.7MPa,伸长率为8.9%。电化学实验和浸泡试验表明,热加工工艺可大幅提高WE43合金的耐腐蚀性。热轧合金具有最佳耐腐蚀性,其腐蚀速率为0.1556±0.18mm/年。