一种生产克级O标记芳香醛的经济有效方法。
A Cost-Effective Way to Produce Gram-Scale O-Labeled Aromatic Aldehydes.
作者信息
Yang Yuan, Han Bingyang, Dong Fenghao, Lv Jiawei, Lu Huiming, Sun Yuqing, Lei Ziqiang, Yang Zengming, Ma Hengchang
机构信息
Key Laboratory of Eco-functional Polymer Materials of the Ministry of Education, Key Laboratory of Eco-environmental Polymer Materials of Gansu Province, College of Chemistry and Chemical Engineering, Northwest Normal University, Lanzhou 730070, China.
出版信息
Org Lett. 2022 Jun 24;24(24):4409-4414. doi: 10.1021/acs.orglett.2c01637. Epub 2022 Jun 14.
Obtaining O-labeled organic substances is of great research importance and also an extremely challenging work. In this work, depending on the reversed Knoevenagel reaction, O-labeled aromatic aldehydes () are successfully obtained with high total yields (52-72%) and sufficient O abundance (90.90-96.09%).
获得氧标记的有机物质具有重大的研究意义，同时也是一项极具挑战性的工作。在这项工作中，依靠逆克诺文纳盖尔反应，成功获得了总产率较高（52 - 72%）且氧丰度充足（90.90 - 96.09%）的氧标记芳香醛（）。
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