在半导体载体上辐照-暗光化学沉积和金属纳米团簇的特性研究方案。
Protocol on irradiation-dark photochemical deposition and characterization of metal nanoclusters on semiconductor support.
机构信息
Research Center of Nano Science and Technology, College of Sciences, Shanghai University, Shanghai 200444, P. R. China.
Research Center of Nano Science and Technology, College of Sciences, Shanghai University, Shanghai 200444, P. R. China; Emerging Industries Institute, Shanghai University, Jiaxing, Zhejiang 314006, P. R. China.
出版信息
STAR Protoc. 2022 Jun 15;3(3):101459. doi: 10.1016/j.xpro.2022.101459. eCollection 2022 Sep 16.
Controlling the size and uniform dispersion of noble metal nanoclusters on the metal oxide based semiconductor are difficult due to the natural tendency for metal atoms to agglomerate. Here, we present the protocol for an "irradiation-dark" photochemical deposition to obtain uniform metal nanoclusters on semiconductor support, and the protocol for measuring the size and size distribution of metal nanoclusters. For complete details on the use and execution of this protocol, please refer to Wu et al. (2022).
由于金属原子自然倾向于团聚，因此控制贵金属纳米团簇在基于金属氧化物的半导体上的尺寸和均匀分散性具有一定难度。在此，我们提供了一种“辐照-暗”光化学沉积方案，用于在半导体载体上获得均匀的金属纳米团簇，以及测量金属纳米团簇尺寸和尺寸分布的方案。如需了解该方案使用和实施的完整详细信息，请参见 Wu 等人（2022 年）。
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