Wilson T D
J Chromatogr. 1987 Apr 3;391(2):409-18. doi: 10.1016/s0021-9673(01)94342-0.
A reversed-phase high-performance liquid chromatographic method has been applied utilizing ion-pairing to measure Tornalate in solution dosage forms. Specificity of the method was demonstrated by selectivity for Tornalate analysis, analysis of stressed samples and by peak homogeneity tests. These included the diode-array derived spectral overlay test and fraction collection with rechromatography in an alternate normal phase system. Linearity was also demonstrated in terms of recovery from synthetic samples and detector response.
已应用一种反相高效液相色谱法，利用离子对来测定溶液剂型中的喘乐宁。该方法的特异性通过对喘乐宁分析的选择性、对强制降解样品的分析以及峰纯度测试得以证明。这些测试包括二极管阵列衍生的光谱叠加测试以及在交替的正相系统中进行馏分收集和重新色谱分析。还通过合成样品的回收率和检测器响应证明了线性关系。
