Cheng Hao, Yan Peihui, Wan Fei, Feng Chao, Zhu Yunfei, Lv Ping, Ma Mingliang
School of Civil Engineering, Qingdao University of Technology, Qingdao 266033, China.
David International Design Institute of Shandong, Jinan 250014, China.
Materials (Basel). 2022 Jul 11;15(14):4827. doi: 10.3390/ma15144827.
In this paper, cement based on fused silica powder @ polyurethane urea (FSP@PUU) with a micro constrained damping structure was studied. Firstly, FSP@PUU core-shell particles were prepared by heterogeneous stepwise addition polymerization method and added into cement paste as damping filler to form a micro-constrained damping structure inside cement paste. The mechanical property and damping performance of cement-based composites were characterized by compressive strength, dynamic mechanical analysis (DMA) test and modal vibration test. The results showed that the damping performance of FSP @ PUU cement-based composites was affected by temperature, and the loss tangent of cement with 6wt% FSP@PUU increased to about 0.057 at -35 °C to 35 °C, which was 1.5 times cement paste within the glass transition temperature. With 6 wt% FSP@PUU, the damping ratio of cement-based composites increased by 58% compared with cement paste in the frequency range of 175-300 Hz, while the compressive strength decreased by only 5%. The cement with suitable FSP@PUU possesses excellent damping performance.
本文研究了具有微约束阻尼结构的基于熔融石英粉@聚氨酯脲(FSP@PUU)的水泥。首先,通过非均相逐步加成聚合法制备FSP@PUU核壳颗粒,并将其作为阻尼填料添加到水泥浆体中,在水泥浆体内形成微约束阻尼结构。通过抗压强度、动态力学分析(DMA)试验和模态振动试验对水泥基复合材料的力学性能和阻尼性能进行了表征。结果表明,FSP@PUU水泥基复合材料的阻尼性能受温度影响,含6wt%FSP@PUU的水泥在-35℃至35℃时损耗角正切增加到约0.057,是玻璃化转变温度范围内水泥浆体的1.5倍。含6wt%FSP@PUU时,在175-300Hz频率范围内,水泥基复合材料的阻尼比与水泥浆体相比提高了58%,而抗压强度仅降低了5%。具有合适FSP@PUU的水泥具有优异的阻尼性能。